Technology Process of 2(3H)-Furanone, dihydro-5-propyl-, (R)-
There total 6 articles about 2(3H)-Furanone, dihydro-5-propyl-, (R)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) sodium metaperiodate, ruthenium trichloride * 3H2O / 1.) carbon tetrachloride, acetonitrile, water, room temperature, 1.5 h; 2.) ether, 3 h
3: 6 h / Irradiation
4: 4-(dimethylamino)pyridine / pyridine / 18 h / Ambient temperature
5: hydrogen / Pd
6: 1.) KOH; 2.) p-toluenesulfonic acid / 1.) EtOH, reflux, 15 min; 2.) benzene,
With
dmap; ruthenium trichloride; potassium hydroxide; sodium periodate; hydrogen; toluene-4-sulfonic acid;
palladium;
In
pyridine;
- Guidance literature:
-
With
sodium hydroxide; disodium hydrogenphosphate; porcine pancreating lipase;
In
diethyl ether; hexane;
at 20 ℃;
for 120h;
pH=7.2;
DOI:10.1016/S0040-4039(02)01268-6
- Guidance literature:
-
With
Glycine max p83 reductase; NADPH;
In
phosphate buffer;
at 36 ℃;
for 5h;
pH=7.0;
Title compound not separated from byproducts;
DOI:10.1016/j.tetlet.2006.12.126