2-Azido-5-chloro-N-(4-chlorophenyl)benzamide

Base Information

Chemical Name:2-Azido-5-chloro-N-(4-chlorophenyl)benzamide
CAS No.:88279-13-4
Molecular Formula:C₁₃H₈Cl₂N₄O
Molecular Weight:307.139
Hs Code.:
DSSTox Substance ID:DTXSID30521495
Wikidata:Q82385993

Synonyms:2-Azido-5-chloro-N-(4-chlorophenyl)benzamide;88279-13-4;DTXSID30521495

Suppliers and Price of 2-Azido-5-chloro-N-(4-chlorophenyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Azido-5-chloro-N-(4-chlorophenyl)benzamide

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:306.0075163
Heavy Atom Count:20
Complexity:392

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1NC(=O)C2=C(C=CC(=C2)Cl)N=[N+]=[N-])Cl

Technology Process of 2-Azido-5-chloro-N-(4-chlorophenyl)benzamide

There total 3 articles about 2-Azido-5-chloro-N-(4-chlorophenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88279-11-2
2-carboxy-4-chlorophenyl azide

: 88279-13-4
2-Azido-5-chloro-N-(4-chloro-phenyl)-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 2 h / Heating

2: pyridine / 0.5 h / Ambient temperature

With pyridine; thionyl chloride;

Reference yield:

: 635-21-2
5-chloroanthranilic acid

: 88279-13-4
2-Azido-5-chloro-N-(4-chloro-phenyl)-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) conc. HCl, NaNO₂, 2.) NaN₃, NaOAc / 1.) water, <5 deg C

2: SOCl₂ / 2 h / Heating

3: pyridine / 0.5 h / Ambient temperature

With pyridine; hydrogenchloride; thionyl chloride; sodium azide; sodium acetate; sodium nitrite;