1-(4-nitrophenyl)imidazolidin-2-one

Base Information

• Chemical Name: 1-(4-nitrophenyl)imidazolidin-2-one
• CAS No.: 89518-83-2
• Molecular Formula: C9H9N3O3
• Molecular Weight: 207.189
• Hs Code.: 2933990090
• Mol file: 89518-83-2.mol

Synonyms:2-Oxo-1-<4-nitro-phenyl>-imidazolidin;1-(4-nitro-phenyl)-imidazolidin-2-one;1-(4-Nitro-phenyl)-imidazolidinon-(2);1-(4-nitrophenyl)-2-imidazolidinone;1-(p-nitrophenyl)-2-imidazolidinone;

Chemical Property of 1-(4-nitrophenyl)imidazolidin-2-one

Chemical Property:

• PKA: 13.40±0.20(Predicted)
• PSA: 78.16000
• Density: 1.396g/cm³
• LogP: 2.04140

Purity/Quality:

99%, ^*data from raw suppliers

1-(4-Nitrophenyl)imidazolidin-2-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-nitrophenyl)imidazolidin-2-one

There total 5 articles about 1-(4-nitrophenyl)imidazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

imidazolidone (120-93-4) + p-nitrobenzene iodide (636-98-6) → 1-(4-nitrophenyl)-imidazolidin-2-one (89518-83-2)

Guidance literature:

With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; In butan-1-ol; at 100 ℃; for 5h;

DOI:10.1016/j.tetlet.2010.04.064

Reference yield:

1-chloroethyl isocyanate (72866-60-5) + N-(2-chloro-ethyl)-N'-(4-nitro-phenyl)-urea (67052-23-7) + 4-nitro-aniline (100-01-6,104810-17-5) → 1-(4-nitrophenyl)-imidazolidin-2-one (89518-83-2)

Guidance literature:

With sodium methylate; In N-methyl-acetamide; methanol; 1,2-dimethoxyethane; ethanol; water; ethyl acetate; toluene;

Reference yield:

1-(2-hydroxyethyl)-3-(4-nitrophenyl)urea (150847-03-3) → 1-(4-nitrophenyl)-imidazolidin-2-one (89518-83-2) + (4,5-Dihydro-oxazol-2-yl)-(4-nitro-phenyl)-amine

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 0.583333h;

DOI:10.1080/00397919908086441

upstream raw materials:

1-(2-hydroxyethyl)-3-(4-nitrophenyl)urea

4-Nitrophenyl isocyanate

1-chloroethyl isocyanate

N-(2-chloro-ethyl)-N'-(4-nitro-phenyl)-urea

Downstream raw materials:

1-(4-aminophenyl)-2-imidazolidinone

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