Benzenetetradecanoic acid, ethyl ester

Base Information

Chemical Name:Benzenetetradecanoic acid, ethyl ester
CAS No.:88336-97-4
Molecular Formula:C22H36O2
Molecular Weight:332.527
Hs Code.:

Synonyms:

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Chemical Property of Benzenetetradecanoic acid, ethyl ester

Chemical Property:

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Technology Process of Benzenetetradecanoic acid, ethyl ester

There total 9 articles about Benzenetetradecanoic acid, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 64-17-5
ethanol

: 88336-96-3
1-(4,4-dimethyl-2-oxazolin-2-yl)-13-phenyltridecane

: 88336-97-4
ethyl 14-phenyltetradecanoate

Guidance literature:: With sulfuric acid; for 24h; Heating;
DOI:10.1021/jm00369a027

Reference yield:

: 2834-05-1
11-bromoundecanoic acid

: 88336-97-4
ethyl 14-phenyltetradecanoate

Guidance literature:: Multi-step reaction with 9 steps

1: SOCl₂ / dimethylformamide / 1 h / 80 °C

2: AlCl₃ / dimethylformamide / 1 h / 90 °C

3: 85 percent / dimethylsulfoxide / 2 h / 80 °C

4: 95 percent / NH₂NH₂*H₂O, KOH / bis-(2-hydroxy-ethyl) ether / 4 h / Heating

5: 95 percent / diethyl ether / 12 h / 0 °C

6: 90 percent / LiAlH₄ / diethyl ether / 4 h / Heating

7: 88 percent / Me₃SiI / CH₂Cl₂ / 24 h / Ambient temperature

8: 1.) n-BuLi / 1.) THF, -78 deg C, 2.) THF, a) -78 deg C, 10 min, b) from -78 deg C to RT

9: 86 percent / concd H₂SO₄ / 24 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; thionyl chloride; trimethylsilyl iodide; sulfuric acid; hydrazine hydrate; In diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; diethylene glycol;
DOI:10.1021/jm00369a027

Reference yield:

: 15949-84-5
11-bromoundecanoyl chloride

: 88336-97-4
ethyl 14-phenyltetradecanoate

Guidance literature:: Multi-step reaction with 8 steps

1: AlCl₃ / dimethylformamide / 1 h / 90 °C

2: 85 percent / dimethylsulfoxide / 2 h / 80 °C

3: 95 percent / NH₂NH₂*H₂O, KOH / bis-(2-hydroxy-ethyl) ether / 4 h / Heating

4: 95 percent / diethyl ether / 12 h / 0 °C

5: 90 percent / LiAlH₄ / diethyl ether / 4 h / Heating

6: 88 percent / Me₃SiI / CH₂Cl₂ / 24 h / Ambient temperature

7: 1.) n-BuLi / 1.) THF, -78 deg C, 2.) THF, a) -78 deg C, 10 min, b) from -78 deg C to RT

8: 86 percent / concd H₂SO₄ / 24 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; trimethylsilyl iodide; sulfuric acid; hydrazine hydrate; In diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; diethylene glycol;
DOI:10.1021/jm00369a027