4-Morpholinecarboxylic acid, 5-[(1S,2S)-2-(acetylamino)-1-hydroxy-3-(3-hydroxyphenyl)propyl]-2-(2,2 -dimethylpropoxy)-3-methyl-, 1,1-dimethylethyl ester, (2R,3S,5R)-

Base Information

• Chemical Name: 4-Morpholinecarboxylic acid, 5-[(1S,2S)-2-(acetylamino)-1-hydroxy-3-(3-hydroxyphenyl)propyl]-2-(2,2 -dimethylpropoxy)-3-methyl-, 1,1-dimethylethyl ester, (2R,3S,5R)-
• CAS No.: 883440-96-8
• Molecular Formula: C26H42N2O7
• Molecular Weight: 494.629

Synonyms:

Chemical Property of 4-Morpholinecarboxylic acid, 5-[(1S,2S)-2-(acetylamino)-1-hydroxy-3-(3-hydroxyphenyl)propyl]-2-(2,2 -dimethylpropoxy)-3-methyl-, 1,1-dimethylethyl ester, (2R,3S,5R)-

Chemical Property:

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Technology Process of 4-Morpholinecarboxylic acid, 5-[(1S,2S)-2-(acetylamino)-1-hydroxy-3-(3-hydroxyphenyl)propyl]-2-(2,2 -dimethylpropoxy)-3-methyl-, 1,1-dimethylethyl ester, (2R,3S,5R)-

There total 1 articles about 4-Morpholinecarboxylic acid, 5-[(1S,2S)-2-(acetylamino)-1-hydroxy-3-(3-hydroxyphenyl)propyl]-2-(2,2 -dimethylpropoxy)-3-methyl-, 1,1-dimethylethyl ester, (2R,3S,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(R)-[2-(S)-amino-1-(S)-hydroxy-3-(3-hydroxyphenyl)-propyl]-2-(R)-(2,2-dimethylpropoxy)-3-(S)-methylmorpholine-4-carboxylic acid tert-butyl ester (883440-87-7) + acetic anhydride (108-24-7) → (2R,3S,5R)-5-[(1S,2S)-2-acetylamino-1-hydroxy-3-(3-hydroxy-phenyl)-propyl]-2-(2,2-dimethyl-propoxy)-3-methyl-morpholine-4-carboxylic acid tert-butyl ester (883440-96-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; for 2.5h;

Reference yield: 80.0%

1-bromo-butane (109-65-9) + (2R,3S,5R)-5-[(1S,2S)-2-acetylamino-1-hydroxy-3-(3-hydroxy-phenyl)-propyl]-2-(2,2-dimethyl-propoxy)-3-methyl-morpholine-4-carboxylic acid tert-butyl ester (883440-96-8) → 5-(R)-[2-(S)-acetylamino-3-(3-butoxyphenyl)-1-(S)-hydroxypropyl]-2-(R)-(2,2-dimethylpropoxy)-3-(S)-methylmorpholine-4-carboxylic acid tert-butyl ester (883440-89-9)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 3h;

Reference yield:

(2R,3S,5R)-5-[(1S,2S)-2-acetylamino-1-hydroxy-3-(3-hydroxy-phenyl)-propyl]-2-(2,2-dimethyl-propoxy)-3-methyl-morpholine-4-carboxylic acid tert-butyl ester (883440-96-8) → N-[(1S,2S)-2-[(3R,5S,6R)-6-(2,2-dimethyl-propoxy)-5-methyl-morpholin-3-yl]-2-hydroxy-1-(3-hydroxy-benzyl)-ethyl]-acetamide trifluoroacetate

Guidance literature:

With trifluoroacetic acid; for 0.666667h;

upstream raw materials:

5-(R)-[2-(S)-amino-1-(S)-hydroxy-3-(3-hydroxyphenyl)-propyl]-2-(R)-(2,2-dimethylpropoxy)-3-(S)-methylmorpholine-4-carboxylic acid tert-butyl ester

acetic anhydride

Downstream raw materials:

5-(R)-[2-(S)-acetylamino-3-(3-butoxyphenyl)-1-(S)-hydroxypropyl]-2-(R)-(2,2-dimethylpropoxy)-3-(S)-methylmorpholine-4-carboxylic acid tert-butyl ester

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