2-Bromo-4-[(Z)-(3-bromo-4-methylphenyl)-NNO-azoxy]-1-methylbenzene

Base Information

• Chemical Name: 2-Bromo-4-[(Z)-(3-bromo-4-methylphenyl)-NNO-azoxy]-1-methylbenzene
• CAS No.: 76274-02-7
• Molecular Formula: C₁₄H₁₂Br₂N₂O
• Molecular Weight: 384.07
• NSC Number: 190825
• DSSTox Substance ID: DTXSID60307365

Synonyms:76274-02-7;2-Bromo-4-[(Z)-(3-bromo-4-methylphenyl)-NNO-azoxy]-1-methylbenzene;NSC190825;DTXSID60307365;NSC-190825;(3-bromo-4-methylphenyl)-(3-bromo-4-methylphenyl)imino-oxidoazanium;AC1L71W0

Chemical Property of 2-Bromo-4-[(Z)-(3-bromo-4-methylphenyl)-NNO-azoxy]-1-methylbenzene

Chemical Property:

• Vapor Pressure: 1.45E-08mmHg at 25°C
• Boiling Point: 470.3°Cat760mmHg
• Flash Point: 238.2°C
• Density: 1.61g/cm³
• XLogP3: 5.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 383.92959
• Heavy Atom Count: 19
• Complexity: 337

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=C(C=C1)N=[N+](C2=CC(=C(C=C2)C)Br)[O-])Br

Technology Process of 2-Bromo-4-[(Z)-(3-bromo-4-methylphenyl)-NNO-azoxy]-1-methylbenzene

There total 2 articles about 2-Bromo-4-[(Z)-(3-bromo-4-methylphenyl)-NNO-azoxy]-1-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-bromo-4-nitrotoluene (7745-93-9) → 3,3'-dibromo-4,4'-dimethylazoxybenzene (76274-02-7)

Guidance literature:

2-bromo-4-nitrotoluene; With sodium tetrahydroborate; palladium diacetate; In ethanol; dichloromethane; water; at 20 ℃;

With oxygen; In ethanol; dichloromethane; water;

DOI:10.1039/c9gc03957k

Reference yield:

3-bromo-4-methylaniline (7745-91-7) → (Z)-1,2-bis(3-bromo-4-methylphenyl)diazene 1-oxide (76274-02-7)

Guidance literature:

With selenium(IV) oxide; dihydrogen peroxide; In methanol; at 20 ℃; Inert atmosphere;

DOI:10.1021/acs.orglett.7b00982

upstream raw materials:

3-bromo-4-methylaniline

2-bromo-4-nitrotoluene

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