N,N-diethyl-2,3,4-trimethoxybenzamide

Base Information

Chemical Name:N,N-diethyl-2,3,4-trimethoxybenzamide
CAS No.:88440-82-8
Molecular Formula:C14H21NO4
Molecular Weight:267.325
Hs Code.:
DSSTox Substance ID:DTXSID10566349
Wikidata:Q82451936

Synonyms:N,N-diethyl-2,3,4-trimethoxybenzamide;88440-82-8;DTXSID10566349;AKOS008917615

Suppliers and Price of N,N-diethyl-2,3,4-trimethoxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diethyl-2,3,4-trimethoxybenzamide

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:267.14705815
Heavy Atom Count:19
Complexity:281

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=C(C(=C(C=C1)OC)OC)OC

Technology Process of N,N-diethyl-2,3,4-trimethoxybenzamide

There total 2 articles about N,N-diethyl-2,3,4-trimethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7169-07-5
3,4,5-(trimethoxy)benzoyl chloride

: 109-89-7
diethylamine

: 88440-82-8
N,N-diethyl-2,3,4-trimethoxybenzamide

Guidance literature:: In dichloromethane; for 3h; Yield given; Ambient temperature;

Reference yield:

: 573-11-5
2,3,4-Trimethoxy-benzoic acid

: 88440-82-8
N,N-diethyl-2,3,4-trimethoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂

2: CH₂Cl₂ / 3 h / Ambient temperature

With thionyl chloride; In dichloromethane;

Reference yield: 85.0%

: 88440-82-8
N,N-diethyl-2,3,4-trimethoxybenzamide

: N,N-diethyl-2,3,4-trimethoxy-5-iodobenzamide

Guidance literature:: With N-iodo-succinimide; silver(I) triflimide; In dichloromethane; at 45 ℃; for 6h; Darkness;
DOI:10.1021/acs.joc.5b02761