Benzoic acid,4-[(cyclopropylcarbonyl)amino]-, ethyl ester

Base Information

• Chemical Name: Benzoic acid,4-[(cyclopropylcarbonyl)amino]-, ethyl ester
• CAS No.: 14372-26-0
• Molecular Formula: C13H15 N O3
• Molecular Weight: 233.2631
• Mol file: 14372-26-0.mol

Synonyms:Benzoicacid, p-cyclopropanecarboxamido-, ethyl ester (8CI); NSC 213648

Chemical Property of Benzoic acid,4-[(cyclopropylcarbonyl)amino]-, ethyl ester

Chemical Property:

• Vapor Pressure: 1.32E-07mmHg at 25°C
• Boiling Point: 430.2°C at 760 mmHg
• Flash Point: 214°C
• PSA: 55.40000
• Density: 1.252g/cm³
• LogP: 2.28480

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid,4-[(cyclopropylcarbonyl)amino]-, ethyl ester

There total 2 articles about Benzoic acid,4-[(cyclopropylcarbonyl)amino]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

cyclopropanecarboxylic acid chloride (4023-34-1) + p-aminoethylbenzoate (94-09-7) → 4-(Cyclopropanecarbonyl-amino)-benzoic acid ethyl ester (14372-26-0)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1016/j.tetlet.2008.12.113

Reference yield:

→ 4-(Cyclopropanecarbonyl-amino)-benzoic acid ethyl ester (14372-26-0)

Guidance literature:

entspr. Amin, Acylierung;

Reference yield: 98.0%

2-methylthio-4-methylpyrimidine (14001-63-9) + 4-(Cyclopropanecarbonyl-amino)-benzoic acid ethyl ester (14372-26-0) → C17H17N3O2S (1142275-06-6)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 10 ℃;

DOI:10.1016/j.tetlet.2008.12.113

upstream raw materials:

cyclopropanecarboxylic acid chloride

p-aminoethylbenzoate

Downstream raw materials:

C₁₇H₁₇N₃O₂S

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