Phenazine, 2-methoxy-, 10-oxide

Base Information

Chemical Name:Phenazine, 2-methoxy-, 10-oxide
CAS No.:2876-29-1
Molecular Formula:C₁₃H₁₀N₂O₂
Molecular Weight:226.235
Hs Code.:
NSC Number:21668
DSSTox Substance ID:DTXSID30182944
Wikidata:Q83053670
ChEMBL ID:CHEMBL1719807
Mol file:2876-29-1.mol

Synonyms:MLS002638803;SMR001548268;2876-29-1;Phenazine, 2-methoxy-, 10-oxide;NSC21668;2-methoxy-10-oxidophenazin-10-ium;Cambridge id 5141537;2-methoxyphenazine 10-oxide;CBDivE_004629;Phenazine,2-methoxy-10-oxide;cid_137753;CHEMBL1719807;SCHEMBL15010394;BDBM91373;DTXSID30182944;HMS3086L09;NSC-21668;2-methoxy-10-oxido-phenazin-10-ium;AKOS003625421;2-methoxy-10-oxidanidyl-phenazin-10-ium;VU0005714-2;SR-01000196739;SR-01000196739-1

Suppliers and Price of Phenazine, 2-methoxy-, 10-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Phenazine, 2-methoxy-, 10-oxide

Chemical Property:

Vapor Pressure:1.92E-07mmHg at 25°C
Boiling Point:437.4°Cat760mmHg
Flash Point:218.4°C
Density:1.29g/cm³
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:226.074227566
Heavy Atom Count:17
Complexity:274

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC2=[N+](C3=CC=CC=C3N=C2C=C1)[O-]

Technology Process of Phenazine, 2-methoxy-, 10-oxide

There total 7 articles about Phenazine, 2-methoxy-, 10-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 273-09-6
benzofurazan

: 141339-54-0
bis(4-anisyl)iodonium triflate

: 2876-29-1
2-Methoxy-phenazin-10-oxid

Guidance literature:: With copper(I) bromide; In 1,2-dichloro-ethane; at 70 ℃; for 24h; regioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01748

Reference yield:

: 88-74-4
2-nitro-aniline

: 2876-29-1
2-Methoxy-phenazin-10-oxid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide; sodium hypochlorite / ethanol; water / 0 °C / Sealed tube; Inert atmosphere

2: triethyl phosphite / tetrahydrofuran / 7 h / 60 °C / Inert atmosphere; Sealed tube

3: copper(I) bromide / 1,2-dichloro-ethane / 24 h / 70 °C / Sealed tube; Inert atmosphere

With sodium hypochlorite; potassium hydroxide; copper(I) bromide; triethyl phosphite; In tetrahydrofuran; ethanol; water; 1,2-dichloro-ethane;
DOI:10.1021/acs.orglett.8b01748

Reference yield:

: 480-96-6,68100-26-5
benzofurazan oxide

: 2876-29-1
2-Methoxy-phenazin-10-oxid

Guidance literature:: Multi-step reaction with 2 steps

1: triethyl phosphite / tetrahydrofuran / 7 h / 60 °C / Inert atmosphere; Sealed tube

2: copper(I) bromide / 1,2-dichloro-ethane / 24 h / 70 °C / Sealed tube; Inert atmosphere

With copper(I) bromide; triethyl phosphite; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/acs.orglett.8b01748