3-PERFLUOROOCTYL-2-IODOPROPANOL

Base Information

• Chemical Name: 3-PERFLUOROOCTYL-2-IODOPROPANOL
• CAS No.: 38550-45-7
• Molecular Formula: C11H6 F17 I O
• Molecular Weight: 604.045
• Hs Code.: 2905590090
• Mol file: 38550-45-7.mol

Synonyms:2-Iodo-1-perfluorooctyl-3-propanol;2-Iodo-3-perfluorooctylpropanol; 3-(Perfluorooctyl)propyleneiodohydrin;4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-2-iodo-1-undecanol;Heptadecafluoro-2-iodo-1-undecanol

Chemical Property of 3-PERFLUOROOCTYL-2-IODOPROPANOL

Chemical Property:

• Vapor Pressure: 0.00401mmHg at 25°C
• Melting Point: 54 °C
• Boiling Point: 248.1 °C at 760 mmHg
• Flash Point: 103.8 °C
• PSA: 20.23000
• Density: 1.888 g/cm³
• LogP: 6.18180

Purity/Quality:

99%, ^*data from raw suppliers

2-Iodo-1H,1H,2H,3H,3H-perfluoroundecan-1-ol 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-PERFLUOROOCTYL-2-IODOPROPANOL

There total 1 articles about 3-PERFLUOROOCTYL-2-IODOPROPANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-iodoheptadecafluorooctane (507-63-1) + allyl alcohol (107-18-6) → 3-perfluoro-n-octyl-2-iodo-1-propanol (38550-45-7)

Guidance literature:

With benzophenone; In methanol; at 20 ℃; for 2h; Reagent/catalyst; Solvent; Irradiation; Inert atmosphere;

DOI:10.1002/adsc.201600501

Reference yield: 88.0%

3-perfluoro-n-octyl-2-iodo-1-propanol (38550-45-7) → 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecan-1-ol (1651-41-8)

Guidance literature:

With tri-n-butyl-tin hydride;

DOI:10.1021/jo990134z

Reference yield: 22.0%

3-perfluoro-n-octyl-2-iodo-1-propanol (38550-45-7) → 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecan-1-ol (1651-41-8) + 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundec-1-ene (61589-64-8)

Guidance literature:

With zinc; In ethylene glycol; at 140 ℃; for 1h;

DOI:10.1016/j.jfluchem.2008.01.012

upstream raw materials:

1-iodoheptadecafluorooctane

allyl alcohol

Downstream raw materials:

(2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluorononyl)oxirane

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecan-1-ol

3-(perfluorooctyl)propyl iodide

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoic acid

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