1-Propanone, (2,4-dinitrophenyl)hydrazone

Base Information

Chemical Name:1-Propanone, (2,4-dinitrophenyl)hydrazone
CAS No.:3375-37-9
Molecular Formula:C15H14N4O4
Molecular Weight:314.301
Hs Code.:
NSC Number:403222
DSSTox Substance ID:DTXSID20419675

Synonyms:MLS003171534;3375-37-9;NSC403222;1-Propanone, 1-phenyl-, (2,4-dinitrophenyl)hydrazone;DTXSID20419675;NSC-403222;1-Propanone, (2,4-dinitrophenyl)hydrazone

Suppliers and Price of 1-Propanone, (2,4-dinitrophenyl)hydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 1-Propanone, (2,4-dinitrophenyl)hydrazone

Chemical Property:

Vapor Pressure:7.76E-09mmHg at 25°C
Boiling Point:465.3°Cat760mmHg
Flash Point:235.2°C
Density:1.32g/cm³
XLogP3:5.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:314.10150494
Heavy Atom Count:23
Complexity:451

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC(=NNC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-])C2=CC=CC=C2
Isomeric SMILES:CC/C(=N/NC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-])/C2=CC=CC=C2

Technology Process of 1-Propanone, (2,4-dinitrophenyl)hydrazone

There total 5 articles about 1-Propanone, (2,4-dinitrophenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 831-91-4
Benzyl phenyl sulfide

: 3375-37-9
propiophenone-(2,4-dinitro-phenylhydrazone)

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / butyl-lithium / tetrahydrofuran; hexane / 0 - 20 °C

2: 85 percent / butyl-lithium, TMEDA / hexane / 0 °C

3: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / -23 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/P19860000195

Reference yield:

: 67274-35-5,321038-62-4
trimethylsilane

: 3375-37-9
propiophenone-(2,4-dinitro-phenylhydrazone)

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / butyl-lithium, TMEDA / hexane / 0 °C

2: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / -23 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; 3-chloro-benzenecarboperoxoic acid; In hexane; dichloromethane;
DOI:10.1039/P19860000195

Reference yield:

: 100-39-0
benzyl bromide

: 3375-37-9
propiophenone-(2,4-dinitro-phenylhydrazone)

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / ethanol

2: 89 percent / butyl-lithium / tetrahydrofuran; hexane / 0 - 20 °C

3: 85 percent / butyl-lithium, TMEDA / hexane / 0 °C

4: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / -23 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; hexane; dichloromethane;
DOI:10.1039/P19860000195