Methyl 5-(2-bromophenyl)furan-2-carboximidate

Base Information

Chemical Name:Methyl 5-(2-bromophenyl)furan-2-carboximidate
CAS No.:88649-67-6
Molecular Formula:C12H10BrNO2
Molecular Weight:280.121
Hs Code.:
DSSTox Substance ID:DTXSID80600825
Wikidata:Q82497109

Synonyms:88649-67-6;Methyl 5-(2-bromophenyl)furan-2-carboximidate;DTXSID80600825

Suppliers and Price of Methyl 5-(2-bromophenyl)furan-2-carboximidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Methyl 5-(2-bromophenyl)furan-2-carboximidate

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:278.98949
Heavy Atom Count:16
Complexity:259

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=N)C1=CC=C(O1)C2=CC=CC=C2Br

Technology Process of Methyl 5-(2-bromophenyl)furan-2-carboximidate

There total 5 articles about Methyl 5-(2-bromophenyl)furan-2-carboximidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-01-1
furfural

: 88649-67-6
5-(2-Bromo-phenyl)-furan-2-carboximidic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) conc. HCl, NaNO₂, 2.) CuCl₂ dihydrate / 1.) H₂O, 0-5 deg C, 0.5 h, 2.) H₂O

2: 76 percent / NH₂OH*HCl, anhydrous NaOAc / various solvent(s); H₂O / 5 h / Heating

3: 47 percent / Ac₂O / 3 h / Heating

4: 28 g / methanol / Ambient temperature

With hydrogenchloride; hydroxylamine hydrochloride; sodium acetate; acetic anhydride; sodium nitrite; In methanol; water;

Reference yield:

: 58110-57-9
5-(2-bromophenyl)furan-2-carboxaldehyde

: 88649-67-6
5-(2-Bromo-phenyl)-furan-2-carboximidic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / NH₂OH*HCl, anhydrous NaOAc / various solvent(s); H₂O / 5 h / Heating

2: 47 percent / Ac₂O / 3 h / Heating

3: 28 g / methanol / Ambient temperature

With hydroxylamine hydrochloride; sodium acetate; acetic anhydride; In methanol; water;

Reference yield:

: 88649-65-4
5-(2'-bromophenyl)-2-furaldehyde oxime

: 88649-67-6
5-(2-Bromo-phenyl)-furan-2-carboximidic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / Ac₂O / 3 h / Heating

2: 28 g / methanol / Ambient temperature

With acetic anhydride; In methanol;