2-(1-Methylcyclopropyl)ethyl 4-methylbenzenesulfonate

Base Information

Chemical Name:2-(1-Methylcyclopropyl)ethyl 4-methylbenzenesulfonate
CAS No.:63064-32-4
Molecular Formula:C13H18 O3 S
Molecular Weight:254.35
Hs Code.:
NSC Number:250987
DSSTox Substance ID:DTXSID40312174
Wikidata:Q82062548

Synonyms:63064-32-4;NSC 250987;NSC250987;2-(1-methylcyclopropyl)ethyl 4-methylbenzenesulfonate;SCHEMBL19046607;DTXSID40312174;NSC-250987;EN300-7051848;2-(1-methylcyclopropyl)ethyl 4-methylbenzene-1-sulfonate;1-METHYLCYCLOPROPANEETHANOL, 4-METHYLBENZENESULFONATE

Suppliers and Price of 2-(1-Methylcyclopropyl)ethyl 4-methylbenzenesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-(1-Methylcyclopropyl)ethyl 4-methylbenzenesulfonate

Chemical Property:

Vapor Pressure:3.62E-05mmHg at 25°C
Boiling Point:364.1°Cat760mmHg
Flash Point:174°C
Density:1.166g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:254.09766561
Heavy Atom Count:17
Complexity:343

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)OCCC2(CC2)C

Technology Process of 2-(1-Methylcyclopropyl)ethyl 4-methylbenzenesulfonate

There total 4 articles about 2-(1-Methylcyclopropyl)ethyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2-(2,2-dibromo-1-methylcyclopropyl)ethyl 4-methylbenzenesulfonate

: 63064-32-4
2-(1-methylcyclopropyl)ethyl 4-methylbenzenesulfonate

Guidance literature:: With pyridine; sodium tetrahydroborate; 3,4,7,8-Tetramethyl-o-phenanthrolin; nickel(II) acetate tetrahydrate; In tetrahydrofuran; water; at 45 ℃; for 0.5h; under 760.051 Torr; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.202006162

Reference yield:

: 781-03-3
isopentenyl tosylate

: 63064-32-4
2-(1-methylcyclopropyl)ethyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide

2: nickel(II) acetate tetrahydrate; sodium tetrahydroborate; 3,4,7,8-Tetramethyl-o-phenanthrolin; pyridine / water; tetrahydrofuran / 0.5 h / 45 °C / 760.05 Torr / Inert atmosphere; Sealed tube

With pyridine; sodium tetrahydroborate; 3,4,7,8-Tetramethyl-o-phenanthrolin; nickel(II) acetate tetrahydrate; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1002/anie.202006162