3-[(4-Nitrobenzoyl)oxy]-2-(4-nitrophenyl)-1,3-oxazinane

Base Information

Chemical Name:3-[(4-Nitrobenzoyl)oxy]-2-(4-nitrophenyl)-1,3-oxazinane
CAS No.:88690-79-3
Molecular Formula:C17H15N3O7
Molecular Weight:373.322
Hs Code.:
DSSTox Substance ID:DTXSID00525526

Synonyms:88690-79-3;3-[(4-Nitrobenzoyl)oxy]-2-(4-nitrophenyl)-1,3-oxazinane;DTXSID00525526

Suppliers and Price of 3-[(4-Nitrobenzoyl)oxy]-2-(4-nitrophenyl)-1,3-oxazinane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-[(4-Nitrobenzoyl)oxy]-2-(4-nitrophenyl)-1,3-oxazinane

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:4
Exact Mass:373.09099983
Heavy Atom Count:27
Complexity:546

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN(C(OC1)C2=CC=C(C=C2)[N+](=O)[O-])OC(=O)C3=CC=C(C=C3)[N+](=O)[O-]

Technology Process of 3-[(4-Nitrobenzoyl)oxy]-2-(4-nitrophenyl)-1,3-oxazinane

There total 3 articles about 3-[(4-Nitrobenzoyl)oxy]-2-(4-nitrophenyl)-1,3-oxazinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 122-04-3
4-nitro-benzoyl chloride

: 88690-66-8
3-Hydroxy-N-(4-nitrophenylmethylen)-1-propanamin-N-oxid

: 88690-79-3
3-(4-Nitrobenzoyloxy)-2-(4-nitrophenyl)-perhydro-1,3-oxazin

Guidance literature:: With triethylamine; In benzene; at 40 ℃; for 2h;

Reference yield:

: 5433-11-4
N-Benzyliden-3-hydroxy-1-propanamin

: 88690-79-3
3-(4-Nitrobenzoyloxy)-2-(4-nitrophenyl)-perhydro-1,3-oxazin

Guidance literature:: Multi-step reaction with 3 steps

1: peroxyacetic acid / CH₂Cl₂ / 12 h / Ambient temperature

2: 1.) 10percent ethanolic H₂SO₄ 2.) 20percent ethanolic KOH / 1.) room temperature, 24h 2.) room temperature, 24h

3: 81 percent / Et₃N / benzene / 2 h / 40 °C

With peracetic acid; potassium hydroxide; sulfuric acid; triethylamine; In dichloromethane; benzene;

Reference yield:

: 3-(3-Phenyl-oxaziridin-2-yl)-propan-1-ol

: 88690-79-3
3-(4-Nitrobenzoyloxy)-2-(4-nitrophenyl)-perhydro-1,3-oxazin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 10percent ethanolic H₂SO₄ 2.) 20percent ethanolic KOH / 1.) room temperature, 24h 2.) room temperature, 24h

2: 81 percent / Et₃N / benzene / 2 h / 40 °C

With potassium hydroxide; sulfuric acid; triethylamine; In benzene;