[(Non-1-yn-1-yl)sulfanyl]benzene

Base Information

Chemical Name:[(Non-1-yn-1-yl)sulfanyl]benzene
CAS No.:88695-37-8
Molecular Formula:C15H20S
Molecular Weight:232.39
Hs Code.:
DSSTox Substance ID:DTXSID90524780
Nikkaji Number:J2.879.445B
Wikidata:Q82391883

Synonyms:[(Non-1-yn-1-yl)sulfanyl]benzene;88695-37-8;DTXSID90524780

Suppliers and Price of [(Non-1-yn-1-yl)sulfanyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of [(Non-1-yn-1-yl)sulfanyl]benzene

Chemical Property:

XLogP3:6.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:7
Exact Mass:232.12857181
Heavy Atom Count:16
Complexity:214

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCC#CSC1=CC=CC=C1

Technology Process of [(Non-1-yn-1-yl)sulfanyl]benzene

There total 5 articles about [(Non-1-yn-1-yl)sulfanyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 3452-09-3
1-nonyne

: 882-33-7
diphenyldisulfane

: 88695-37-8
non-1-yn-1-yl(phenyl)sulfane

Guidance literature:: With copper; oxygen; sodium carbonate; In dimethyl sulfoxide; at 70 ℃; for 12h; under 1520.1 Torr; Autoclave; Green chemistry;
DOI:10.1055/s-0035-1560458

Reference yield:

: 3452-09-3
1-nonyne

: 882-33-7
diphenyldisulfane

: 100-68-5
methyl-phenyl-thioether

: 88695-37-8
non-1-yn-1-yl(phenyl)sulfane

Guidance literature:: With n-butyllithium; methyl iodide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 30 min, 2.) THF, r.t, 1 h;

Reference yield:

: 148237-55-2
Trimethyl-((Z)-1-phenylsulfanyl-non-1-enyl)-silane

: 88695-37-8
non-1-yn-1-yl(phenyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1: MCPBA

2: 2.) p-TsOH / 1.) benzene, reflux, 10 h 2.) methanol, 60 min.

With 3-chloro-benzenecarboperoxoic acid; toluene-4-sulfonic acid;
DOI:10.1016/S0040-4039(00)85904-3