1-(1,3-Dimethyl-3-cyclohexen-1-yl)-2-buten-1-one

Base Information

Chemical Name:1-(1,3-Dimethyl-3-cyclohexen-1-yl)-2-buten-1-one
CAS No.:83258-29-1
Molecular Formula:C₁₂H₁₈O
Molecular Weight:178.274
Hs Code.:
European Community (EC) Number:280-347-4
Nikkaji Number:J326.775J
Mol file:83258-29-1.mol

Synonyms:EINECS 280-347-4;1-(1,3-Dimethyl-3-cyclohexen-1-yl)-2-buten-1-one;83258-29-1;SCHEMBL11147806

Suppliers and Price of 1-(1,3-Dimethyl-3-cyclohexen-1-yl)-2-buten-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1-(1,3-Dimethyl-3-cyclohexen-1-yl)-2-buten-1-one

Chemical Property:

Vapor Pressure:0.0161mmHg at 25°C
Boiling Point:255.7°Cat760mmHg
Flash Point:100.5°C
Density:0.918g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:178.135765193
Heavy Atom Count:13
Complexity:260

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC=CC(=O)C1(CCC=C(C1)C)C
Isomeric SMILES:C/C=C/C(=O)C1(CCC=C(C1)C)C

Technology Process of 1-(1,3-Dimethyl-3-cyclohexen-1-yl)-2-buten-1-one

There total 6 articles about 1-(1,3-Dimethyl-3-cyclohexen-1-yl)-2-buten-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83258-28-0
1(1,4-dimethyl-cyclohex-3-en-1-yl)-but-2-en-1-one

: 83258-29-1
(E)-1-(1,3-dimethyl-3-cyclohexenyl)-2-buten-1-one

Guidance literature:

Reference yield:

: 56146-92-0
methyl 1,3-dimethyl-3-cyclohexenecarboxylate

: 83258-29-1
(Z)-1-(1,3-dimethyl-3-cyclohexenyl)-2-buten-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: Mg / MeI / diethyl ether / 1.) reflux, 2.5 h; 2.) reflux, 3 h

2: t-BuOK / dimethylformamide / 2.5 h / 50 °C

With potassium tert-butylate; magnesium; methyl iodide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19840670124

Reference yield:

: 56146-92-0
methyl 1,3-dimethyl-3-cyclohexenecarboxylate

: 83258-29-1
(E)-1-(1,3-dimethyl-3-cyclohexenyl)-2-buten-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: Mg / MeI / diethyl ether / 1.) reflux, 2.5 h; 2.) reflux, 3 h

2: t-BuOK / dimethylformamide / 2.5 h / 50 °C

With potassium tert-butylate; magnesium; methyl iodide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19840670124