1-Carbomethoxy-1,3-dimethylcyclohex-3-ene

Base Information

Chemical Name:1-Carbomethoxy-1,3-dimethylcyclohex-3-ene
CAS No.:56146-92-0
Molecular Formula:C10H16O2
Molecular Weight:168.236
Hs Code.:
DSSTox Substance ID:DTXSID70486155

Synonyms:1-carbomethoxy-1,3-dimethylcyclohex-3-ene;56146-92-0;DTXSID70486155;ULVFWYLWNCCUDP-UHFFFAOYSA-N;3-Cyclohexene-1-carboxylic acid, 1,3-dimethyl-, methyl ester

Suppliers and Price of 1-Carbomethoxy-1,3-dimethylcyclohex-3-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Carbomethoxy-1,3-dimethylcyclohex-3-ene

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:168.115029749
Heavy Atom Count:12
Complexity:218

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CCCC(C1)(C)C(=O)OC

Technology Process of 1-Carbomethoxy-1,3-dimethylcyclohex-3-ene

There total 2 articles about 1-Carbomethoxy-1,3-dimethylcyclohex-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7
methacrylic acid methyl ester

: 78-79-5,9003-31-0
isoprene

: 58911-05-0,23733-88-2
1,4-Dimethyl-3-cyclohexen-1-carbonsaeure-methylester

: 56146-92-0
methyl 1,3-dimethyl-3-cyclohexenecarboxylate

Guidance literature:: nanoporous Al-HMS; In hexane; at -1 ℃; for 32h;
DOI:10.1246/cl.2002.166

Reference yield:

: 56146-92-0
methyl 1,3-dimethyl-3-cyclohexenecarboxylate

Guidance literature:: 1,5-Dimethylcyclohexen-5-carbonsaeure, CH2N2; Ausb.6percent;
DOI:10.1016/S0040-4020(01)82796-4

Reference yield:

: 56146-92-0
methyl 1,3-dimethyl-3-cyclohexenecarboxylate

: 1-(1,3-dimethyl-3-cyclohexenyl)-3-buten-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: Mg / MeI / diethyl ether / 1.) reflux, 2.5 h; 2.) reflux, 3 h

2: t-BuOK / dimethylformamide / 2.5 h / 50 °C

With potassium tert-butylate; magnesium; methyl iodide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19840670124