4-Piperidinecarboxaldehyde, 1-(phenylmethyl)-, oxime

Base Information

Chemical Name:4-Piperidinecarboxaldehyde, 1-(phenylmethyl)-, oxime
CAS No.:88796-02-5
Molecular Formula:C13H18N2O
Molecular Weight:218.299
Hs Code.:

Synonyms:

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Chemical Property of 4-Piperidinecarboxaldehyde, 1-(phenylmethyl)-, oxime

Chemical Property:

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Technology Process of 4-Piperidinecarboxaldehyde, 1-(phenylmethyl)-, oxime

There total 3 articles about 4-Piperidinecarboxaldehyde, 1-(phenylmethyl)-, oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: C₆H₁₂N₂O*ClH

: 100-52-7
benzaldehyde

: 88796-02-5
1-benzylpiperidine-4-carbaldehyde oxime

Guidance literature:: C₆H₁₂N₂O*ClH; benzaldehyde; With magnesium sulfate; triethylamine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1055/s-0034-1378881

Reference yield:

: 137076-22-3
tert butyl 4-formylpiperidine-1-carboxylate

: 88796-02-5
1-benzylpiperidine-4-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; hydroxylamine hydrochloride / dichloromethane / 16 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C / Inert atmosphere

3.1: triethylamine; magnesium sulfate / dichloromethane / 16 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; hydroxylamine hydrochloride; magnesium sulfate; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1055/s-0034-1378881

Reference yield:

: 190446-85-6
tert-butyl 4-((hydroxyimino)methyl)piperidine-1-carboxylate

: 88796-02-5
1-benzylpiperidine-4-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C / Inert atmosphere

2.1: triethylamine; magnesium sulfate / dichloromethane / 16 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; magnesium sulfate; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1055/s-0034-1378881