Benzene, (1-chloro-5,9-dimethyl-5,9-undecadienyl)-

Base Information

Chemical Name:Benzene, (1-chloro-5,9-dimethyl-5,9-undecadienyl)-
CAS No.:88829-65-6
Molecular Formula:C19H27Cl
Molecular Weight:290.876
Hs Code.:

Synonyms:

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Chemical Property of Benzene, (1-chloro-5,9-dimethyl-5,9-undecadienyl)-

Chemical Property:

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Technology Process of Benzene, (1-chloro-5,9-dimethyl-5,9-undecadienyl)-

There total 12 articles about Benzene, (1-chloro-5,9-dimethyl-5,9-undecadienyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120060-01-7
5,9-dimethyl-1-phenylundeca-5,9-dien-1-ol

: 88829-65-6
11-chloro-3,7-dimethyl-11-phenyl-2,6-undecadiene

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; methyllithium; methanesulfonyl chloride; lithium chloride; Yield given. Multistep reaction; 1.) anhydrous ether, hexamethylphosphoramide, 2.) room temp., 20 min;
DOI:10.1021/jo00269a053

Reference yield:

: 120060-00-6
10-bromo-3,7-dimethyl-2,6-decadiene

: 88829-65-6
11-chloro-3,7-dimethyl-11-phenyl-2,6-undecadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 18.56 percent / lithium; CH₃I / tetrahydrofuran / 0 °C / sonication

2: thionyl chloride / petroleum ether / 2 h / -15 °C / 520 - 560 Torr

With thionyl chloride; lithium; methyl iodide; In tetrahydrofuran; Petroleum ether; 1: Barbier reaction / 2: Chlorination;
DOI:10.1021/jo972237s

Reference yield:

: 57253-27-7
(E)-4-methylhex-4-en-1-ol

: 88829-65-6
11-chloro-3,7-dimethyl-11-phenyl-2,6-undecadiene

Guidance literature:: Multi-step reaction with 5 steps

1: CrO₃, HCl / pyridine

4: LiAlH₄

With chromium(VI) oxide; hydrogenchloride; lithium aluminium tetrahydride; In pyridine;
DOI:10.1039/c39830001044