Technology Process of 5,9-dimethyl-1-phenylundeca-5,9-dien-1-ol
There total 9 articles about 5,9-dimethyl-1-phenylundeca-5,9-dien-1-ol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium; methyl iodide;
In
tetrahydrofuran;
at 0 ℃;
sonication;
DOI:10.1021/jo972237s
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 51 percent / 1.) pyridinium chlorochromate / CH2Cl2 / 1.) 0 deg C, 2.) reflux
2: 1.) magnesium ribbon / 1.) anhydrous THF, 0 deg C, 2.) THF
3: propionic acid / Heating
4: 1.) LiAlH4 / diethyl ether / 1.) 0 deg C, 2.) room temp., 2 h
5: pyridine / 2 h / 0 °C
6: anhydrous LiBr / acetone / 0.5 h / Heating
7: Li / tetrahydrofuran / Ambient temperature
With
pyridine; lithium aluminium tetrahydride; lithium; magnesium; propionic acid; pyridinium chlorochromate; lithium bromide;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetone;
DOI:10.1021/jo00269a053
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) magnesium ribbon / 1.) anhydrous THF, 0 deg C, 2.) THF
2: propionic acid / Heating
3: 1.) LiAlH4 / diethyl ether / 1.) 0 deg C, 2.) room temp., 2 h
4: pyridine / 2 h / 0 °C
5: anhydrous LiBr / acetone / 0.5 h / Heating
6: Li / tetrahydrofuran / Ambient temperature
With
pyridine; lithium aluminium tetrahydride; lithium; magnesium; propionic acid; lithium bromide;
In
tetrahydrofuran; diethyl ether; acetone;
DOI:10.1021/jo00269a053
