Benzoic acid, 2-[(4-chlorobenzoyl)oxy]-

Base Information

• Chemical Name: Benzoic acid, 2-[(4-chlorobenzoyl)oxy]-
• CAS No.: 88875-74-5
• Molecular Formula: C14H9ClO4
• Molecular Weight: 276.676
• Mol file: 88875-74-5.mol

Synonyms:

Chemical Property of Benzoic acid, 2-[(4-chlorobenzoyl)oxy]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 2-[(4-chlorobenzoyl)oxy]-

There total 5 articles about Benzoic acid, 2-[(4-chlorobenzoyl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

potassium 4'-chloroflavonolate → O-(4-chlorobenzoyl)-salicylic acid (88875-74-5)

Guidance literature:

With oxygen; In N,N-dimethyl-formamide; at 50 ℃; for 8h; under 750.075 Torr;

DOI:10.1021/jo991926w

Reference yield: 43.0%

C16H10Cl4O4 (88875-66-5) → O-(4-chlorobenzoyl)-salicylic acid (88875-74-5)

Guidance literature:

With acetic acid; zinc; In tetrahydrofuran; for 0.5h; Ambient temperature;

DOI:10.1248/cpb.31.2632

Reference yield:

3-Hydroxy-4'-chloroflavone (19275-70-8) → O-(4-chlorobenzoyl)-salicylic acid (88875-74-5)

Guidance literature:

With C₃₀H₂₃FeN₂O₆; oxygen; In N,N-dimethyl-formamide; at 100 ℃; for 15h; chemoselective reaction; Activation energy; Kinetics; Mechanism; Thermodynamic data;

DOI:10.1016/j.jinorgbio.2011.11.013

upstream raw materials:

C₁₆H₁₀Cl₄O₄

4-chloro-benzoyl chloride

salicylic acid

2,2,2-trichloroethyl salicylate

Downstream raw materials:

2-(4-chlorophenyl)-3-chloroflavone

C₁₄H₉O₄ClC₆H₁₄Si

4'-chloroflavone