[4-[9-[4-(3-bromobenzoyl)oxyphenyl]-10,10-diphenyl-anthracen-9-yl]phenyl] 3-bromobenzoate

Base Information

• Chemical Name: [4-[9-[4-(3-bromobenzoyl)oxyphenyl]-10,10-diphenyl-anthracen-9-yl]phenyl] 3-bromobenzoate
• CAS No.: 7470-29-3
• Molecular Formula: C₅₂H₃₄Br₂O₄
• Molecular Weight: 882.648
• Mol file: 7470-29-3.mol

Synonyms:

Chemical Property of [4-[9-[4-(3-bromobenzoyl)oxyphenyl]-10,10-diphenyl-anthracen-9-yl]phenyl] 3-bromobenzoate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 52.60000
• Density: 1.426g/cm³
• LogP: 12.72880

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [4-[9-[4-(3-bromobenzoyl)oxyphenyl]-10,10-diphenyl-anthracen-9-yl]phenyl] 3-bromobenzoate

There total 3 articles about [4-[9-[4-(3-bromobenzoyl)oxyphenyl]-10,10-diphenyl-anthracen-9-yl]phenyl] 3-bromobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10.10-Diphenyl-9-(4-hydroxy-phenyl)-9-(4-methoxy-phenyl)-9.10-dihydro-anthracen (857589-50-5) → 9,9-bis-[4-(3-bromo-benzoyloxy)-phenyl]-10,10-diphenyl-9,10-dihydro-anthracene (7470-29-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid; aqueous HBr

2: 190 - 200 °C

With hydrogen bromide; acetic acid;

DOI:10.1021/ja01278a027

Reference yield:

phenol (108-95-2,27073-41-2) → 9,9-bis-[4-(3-bromo-benzoyloxy)-phenyl]-10,10-diphenyl-9,10-dihydro-anthracene (7470-29-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid / auf dem Dampfbad

2: acetic acid; aqueous HBr

3: 190 - 200 °C

With sulfuric acid; hydrogen bromide; acetic acid;

DOI:10.1021/ja01278a027

Reference yield:

3-bromobenzoyl chloride (1711-09-7) + 9,9-bis-(4-hydroxy-phenyl)-10,10-diphenyl-9,10-dihydro-anthracene (7505-38-6) → 9,9-bis-[4-(3-bromo-benzoyloxy)-phenyl]-10,10-diphenyl-9,10-dihydro-anthracene (7470-29-3)

Guidance literature:

at 190 - 200 ℃;

DOI:10.1021/ja01278a027

upstream raw materials:

3-bromobenzoyl chloride

9,9-bis-(4-hydroxy-phenyl)-10,10-diphenyl-9,10-dihydro-anthracene

10.10-Diphenyl-9-(4-hydroxy-phenyl)-9-(4-methoxy-phenyl)-9.10-dihydro-anthracen

phenol