5-chloro-2-methoxy-phenol

Base Information

• Chemical Name: 5-chloro-2-methoxy-phenol
• CAS No.: 3743-23-5
• Molecular Formula: C7H7 Cl O2
• Molecular Weight: 158.584
• Hs Code.: 2909500000
• Mol file: 3743-23-5.mol

Synonyms:Guaiacol,5-chloro- (6CI); 2-Hydroxy-4-chloroanisole; 5-Chloro-2-methoxyphenol;5-Chloroguaiacol

Chemical Property of 5-chloro-2-methoxy-phenol

Chemical Property:

• Vapor Pressure: 0.0286mmHg at 25°C
• Melting Point: 161-163.5℃
• Boiling Point: 237-239℃ (760 Torr)
• Flash Point: 97.6°C
• PSA: 29.46000
• Density: 1.28g/cm³
• LogP: 2.05420
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

5-Chloro-2-methoxyphenol ^*data from reagent suppliers

Safty Information:

• Statements: 41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-chloro-2-methoxy-phenol

There total 12 articles about 5-chloro-2-methoxy-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

5-chloro-2-methoxyphenyl boronic acid (89694-48-4) → 5-chloro-2-methoxyphenol (3743-23-5)

Guidance literature:

With dihydrogen peroxide; In ethanol; at 80 ℃; for 0.5h;

Reference yield: 71.0%

5-chloro-2-methoxybenzaldehyde (7035-09-8) → 5-chloro-2-methoxyphenol (3743-23-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid;

DOI:10.1021/jo00180a019

Reference yield: 54.0%

(5-chloro-2-methoxybenzyl)trimethylsilane → 5-chloro-2-methoxyphenol (3743-23-5)

Guidance literature:

With sodium persulfate; oxygen; In acetonitrile; at 55 ℃; for 12h;

DOI:10.1039/c7cc01868a

upstream raw materials:

5-nitroguaiacol

tetrachloromethane

tert-butylhypochlorite

2-methoxy-phenol

Downstream raw materials:

(5-chloro-2-methoxy-phenoxy)-acetic acid

guaiacol-5-sulfonic acid

2-allyloxy-4-chloro-1-methoxy-benzene

2-(2-Methoxy-5-chlorophenoxy)-3-<2-(N-formamido)ethyl>-2-cyclohexen-1-one

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