4-Acetyl-5-hydroxy-5-methyl-2,3-diphenylcyclopent-2-en-1-one

Base Information

Chemical Name:4-Acetyl-5-hydroxy-5-methyl-2,3-diphenylcyclopent-2-en-1-one
CAS No.:88964-78-7
Molecular Formula:C20H18O3
Molecular Weight:306.361
Hs Code.:
DSSTox Substance ID:DTXSID50525637

Synonyms:88964-78-7;4-Acetyl-5-hydroxy-5-methyl-2,3-diphenylcyclopent-2-en-1-one;DTXSID50525637

Suppliers and Price of 4-Acetyl-5-hydroxy-5-methyl-2,3-diphenylcyclopent-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4-Acetyl-5-hydroxy-5-methyl-2,3-diphenylcyclopent-2-en-1-one

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:306.125594432
Heavy Atom Count:23
Complexity:521

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1C(=C(C(=O)C1(C)O)C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of 4-Acetyl-5-hydroxy-5-methyl-2,3-diphenylcyclopent-2-en-1-one

There total 3 articles about 4-Acetyl-5-hydroxy-5-methyl-2,3-diphenylcyclopent-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 85572-21-0
4-acetyl-5-hydroxy-5-methyl-1-methylthio-2,3-diphenyl-1,3-cyclopentadiene

: 88964-78-7
4-acetyl-5-hydroxy-5-methyl-2,3-diphenyl-2-cyclopentenone

Guidance literature:: With water; trifluoroacetic acid; mercury dichloride; In chloroform; for 72h; Ambient temperature;
DOI:10.1246/bcsj.56.3015

Reference yield:

: 1,2-diphenyl-3-(methylthio)cyclopropenium bromide

: 88964-78-7
4-acetyl-5-hydroxy-5-methyl-2,3-diphenyl-2-cyclopentenone

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Et₃N / benzene / 0.33 h

2: 88 percent / HgCl₂, TFA, H₂O / CHCl₃ / 72 h / Ambient temperature

With water; triethylamine; trifluoroacetic acid; mercury dichloride; In chloroform; benzene;
DOI:10.1246/bcsj.56.3015

Reference yield:

: 2570-01-6
2,3-diphenylcyclopropen-1-thione

: 88964-78-7
4-acetyl-5-hydroxy-5-methyl-2,3-diphenyl-2-cyclopentenone

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / benzene / 48 h / Ambient temperature

2: 73 percent / Et₃N / benzene / 0.33 h

3: 88 percent / HgCl₂, TFA, H₂O / CHCl₃ / 72 h / Ambient temperature

With water; triethylamine; trifluoroacetic acid; mercury dichloride; In chloroform; benzene;
DOI:10.1246/bcsj.56.3015