Acetic acid, (((1-(4-ethyl-3,4-dihydro-3-oxo-2H-1,4-benzothiazin-6-yl)ethylidene)amino)oxy)-,2-(diethylamino)ethyl ester

Base Information

Chemical Name:Acetic acid, (((1-(4-ethyl-3,4-dihydro-3-oxo-2H-1,4-benzothiazin-6-yl)ethylidene)amino)oxy)-,2-(diethylamino)ethyl ester
CAS No.:91119-88-9
Molecular Formula:C₂₀H₂₉N₃O₄S
Molecular Weight:407.534
Hs Code.:

Synonyms:BRN 4589723;Acetic acid, (((1-(4-ethyl-3,4-dihydro-3-oxo-2H-1,4-benzothiazin-6-yl)ethylidene)amino)oxy)-,2-(diethylamino)ethyl ester;91119-88-9;C20H29N3O4S;C20-H29-N3-O4-S

Suppliers and Price of Acetic acid, (((1-(4-ethyl-3,4-dihydro-3-oxo-2H-1,4-benzothiazin-6-yl)ethylidene)amino)oxy)-,2-(diethylamino)ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid, (((1-(4-ethyl-3,4-dihydro-3-oxo-2H-1,4-benzothiazin-6-yl)ethylidene)amino)oxy)-,2-(diethylamino)ethyl ester

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:592°Cat760mmHg
Flash Point:311.8°C
Density:1.19g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:11
Exact Mass:407.18787759
Heavy Atom Count:28
Complexity:554

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN1C(=O)CSC2=C1C=C(C=C2)C(=NOCC(=O)OCCN(CC)CC)C
Isomeric SMILES:CCN1C(=O)CSC2=C1C=C(C=C2)/C(=N/OCC(=O)OCCN(CC)CC)/C

Technology Process of Acetic acid, (((1-(4-ethyl-3,4-dihydro-3-oxo-2H-1,4-benzothiazin-6-yl)ethylidene)amino)oxy)-,2-(diethylamino)ethyl ester

There total 7 articles about Acetic acid, (((1-(4-ethyl-3,4-dihydro-3-oxo-2H-1,4-benzothiazin-6-yl)ethylidene)amino)oxy)-,2-(diethylamino)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 869-24-9
2-chloro-N,N-diethylethylamine hydrochloride

: 91119-87-8
[1-(4-Ethyl-3-oxo-3,4-dihydro-2H-benzo[1,4]thiazin-6-yl)-eth-(E)-ylideneaminooxy]-acetic acid

: 91119-88-9
[1-(4-Ethyl-3-oxo-3,4-dihydro-2H-benzo[1,4]thiazin-6-yl)-eth-(E)-ylideneaminooxy]-acetic acid 2-diethylamino-ethyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 2h; Heating;

Reference yield:

: 5465-65-6
4-chloro-3-nitroacetophenone

: 91119-88-9
[1-(4-Ethyl-3-oxo-3,4-dihydro-2H-benzo[1,4]thiazin-6-yl)-eth-(E)-ylideneaminooxy]-acetic acid 2-diethylamino-ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 60 percent / NaHCO₃ / aq. ethanol / 2 h / Heating

2: 55 percent / FeSO₄*7H₂O / aq. NH₃ / 1 h / Heating

3: 86 percent / KOH / acetone / 5 h / Heating

4: 70 percent / NH₂OH*HCl, pyridine / ethanol / 2 h / Heating

5: 78 percent / aq.NaOH / tetrabutylammonium hydrogen sulphate / 0.5 h / Ambient temperature

6: 85 percent / aq.NaOH / 2 h / Heating

7: 80 percent / Et₃N / dimethylformamide / 2 h / Heating

With pyridine; potassium hydroxide; sodium hydroxide; hydroxylamine hydrochloride; sodium hydrogencarbonate; iron(II) sulfate; triethylamine; tetra(n-butyl)ammonium hydrogensulfate; In ammonium hydroxide; ethanol; N,N-dimethyl-formamide; acetone;

Reference yield:

: 91119-38-9
6-Acetyl-2H-1,4-benzothiazine-3(4H)-one

: 91119-88-9
[1-(4-Ethyl-3-oxo-3,4-dihydro-2H-benzo[1,4]thiazin-6-yl)-eth-(E)-ylideneaminooxy]-acetic acid 2-diethylamino-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / KOH / acetone / 5 h / Heating

2: 70 percent / NH₂OH*HCl, pyridine / ethanol / 2 h / Heating

3: 78 percent / aq.NaOH / tetrabutylammonium hydrogen sulphate / 0.5 h / Ambient temperature

4: 85 percent / aq.NaOH / 2 h / Heating

5: 80 percent / Et₃N / dimethylformamide / 2 h / Heating

With pyridine; potassium hydroxide; sodium hydroxide; hydroxylamine hydrochloride; triethylamine; tetra(n-butyl)ammonium hydrogensulfate; In ethanol; N,N-dimethyl-formamide; acetone;