Benzoic acid, 3-[6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-6-fluoro-11,11-dimethyl- 3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Benzoic acid, 3-[6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-6-fluoro-11,11-dimethyl- 3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester
CAS No.:889857-55-0
Molecular Formula:C31H41ClFN3O7
Molecular Weight:622.134
Hs Code.:

Benzoic acid,
3-[6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-6-fluoro-11,11-dimethyl-
3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester

Synonyms:

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Chemical Property of Benzoic acid, 3-[6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-6-fluoro-11,11-dimethyl- 3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester

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Technology Process of Benzoic acid, 3-[6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-6-fluoro-11,11-dimethyl- 3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester

There total 2 articles about Benzoic acid, 3-[6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-6-fluoro-11,11-dimethyl- 3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 889858-22-4
tert-butyl 3-{1-[(aminocarbonyl)amino]propyl}benzoate

: C₂₃H₂₂Cl₄FNO₆

: 889857-55-0
tert-butyl 3-[6-(5-chloro-2-methoxybenzyl)-1-ethyl-6-fluoro-11,11-dimethyl-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]benzoate

Guidance literature:: With dmap; In toluene; at 20 ℃; for 3h;

Reference yield:

: 889856-09-1
N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine

: 889858-22-4
tert-butyl 3-{1-[(aminocarbonyl)amino]propyl}benzoate

: 4136-95-2
2,4,6-trichlorobenzoyl chloride

: 889857-55-0
tert-butyl 3-[6-(5-chloro-2-methoxybenzyl)-1-ethyl-6-fluoro-11,11-dimethyl-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]benzoate

Guidance literature:: N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine; 2,4,6-trichlorobenzoyl chloride; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 1h;

tert-butyl 3-{1-[(aminocarbonyl)amino]propyl}benzoate; With dmap; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 889857-55-0
tert-butyl 3-[6-(5-chloro-2-methoxybenzyl)-1-ethyl-6-fluoro-11,11-dimethyl-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]benzoate

: 24424-99-5
di-tert-butyl dicarbonate

: 100-51-6,185532-71-2
benzyl alcohol

: 889857-56-1
benzyl 3-[6-(5-chloro-2-methoxybenzyl)-1-ethyl-6-fluoro-11,11-dimethyl-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]benzoate

Guidance literature:: tert-butyl 3-[6-(5-chloro-2-methoxybenzyl)-1-ethyl-6-fluoro-11,11-dimethyl-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]benzoate; With hydrogenchloride; In water; acetic acid; at 20 ℃; for 1h;

di-tert-butyl dicarbonate; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 3h;

benzyl alcohol; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 5h;