N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine
CAS No.:889856-09-1
Molecular Formula:C₁₆H₂₁ClFNO₅
Molecular Weight:361.798
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine

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Chemical Property of N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine

Chemical Property:

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Technology Process of N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine

There total 2 articles about N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₃ClFNO₃

: 24424-99-5
di-tert-butyl dicarbonate

: 889856-09-1
N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine

Guidance literature:: C₁₁H₁₃ClFNO₃; di-tert-butyl dicarbonate; With sodium hydroxide; In tetrahydrofuran; water; ethyl acetate; at 20 ℃; for 4h;

With potassium hydrogensulfate; In tetrahydrofuran; water; ethyl acetate;

Reference yield:

: 889856-07-9
3-azido-2-(5-chloro-2-methoxybenzyl)-2-fluoropropanoic acid

: 24424-99-5
di-tert-butyl dicarbonate

: 889856-09-1
N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine

Guidance literature:: 3-azido-2-(5-chloro-2-methoxybenzyl)-2-fluoropropanoic acid; With water; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 5h;

di-tert-butyl dicarbonate; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 4h;

Reference yield:

: 889856-09-1
N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine

: 4136-95-2
2,4,6-trichlorobenzoyl chloride

: 77207-59-1
((R)-1-phenyl-propyl)-urea

: 889858-21-3
tert-butyl 2-(5-chloro-2-methoxybenzyl)-2-fluoro-3-oxo-3-[({[(1R)-1-phenylpropyl]amino}carbonyl)amino]propylcarbamate

Guidance literature:: N-(tert-butoxycarbonyl)-2-(5-chloro-2-methoxybenzyl)-2-fluoro-β-alanine; 2,4,6-trichlorobenzoyl chloride; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 1.5h;

((R)-1-phenyl-propyl)-urea; In tetrahydrofuran; at 20 ℃; for 3h;