9-Phenanthrenebutanenitrile

Base Information

Chemical Name:9-Phenanthrenebutanenitrile
CAS No.:88986-03-2
Molecular Formula:C18H15N
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID50478437
Nikkaji Number:J2.184.891C
Wikidata:Q82311820

Synonyms:9-Phenanthrenebutanenitrile;88986-03-2;DTXSID50478437

Suppliers and Price of 9-Phenanthrenebutanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 9-Phenanthrenebutanenitrile

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:245.120449483
Heavy Atom Count:19
Complexity:339

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=C(C3=CC=CC=C23)CCCC#N

Technology Process of 9-Phenanthrenebutanenitrile

There total 1 articles about 9-Phenanthrenebutanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 14918-21-9
5-hexynonitrile

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 5661-06-3
2,3-dihydro-1H-cyclopenta[b]quinoline

: 88986-03-2
4-(phenanthren-9-yl)butyronitrile

Guidance literature:: With dibromo[1,2-bis(diphenylphosphino)ethane]nickel(II); cesium fluoride; zinc; In acetonitrile; at 80 ℃; for 12h;
DOI:10.1039/b415691a

Reference yield:

: 88986-03-2
4-(phenanthren-9-yl)butyronitrile

: 88985-95-9
9-(4-anilinobutyl)phenanthrene

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / KOH / ethanol / 20 h / Heating

2: thionyl chloride / 0.17 h / Heating

3: diethyl ether / 4.5 h / Ambient temperature

4: 90 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 3.5 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1246/bcsj.56.3118

Reference yield:

: 88986-03-2
4-(phenanthren-9-yl)butyronitrile

: 1'-phenylspiro<9,10-dihydrophenanthrene-9,2'-piperidine>

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / KOH / ethanol / 20 h / Heating

2: thionyl chloride / 0.17 h / Heating

3: diethyl ether / 4.5 h / Ambient temperature

4: 90 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 3.5 h / Heating

5: 40 percent / acetonitrile / 1.5 h / Irradiation

With potassium hydroxide; lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran; diethyl ether; ethanol; acetonitrile;
DOI:10.1246/bcsj.56.3118