N,N-dimethyl-3-(tributylstannanyl)propan-1-amine

Base Information

Chemical Name:N,N-dimethyl-3-(tributylstannanyl)propan-1-amine
CAS No.:29346-31-4
Molecular Formula:C₁₇H₃₉NSn
Molecular Weight:376.213
Hs Code.:
Mol file:29346-31-4.mol

Synonyms:Propylamine,N,N-dimethyl-3-(tributylstannyl)- (8CI); NSC 294240

Suppliers and Price of N,N-dimethyl-3-(tributylstannanyl)propan-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of N,N-dimethyl-3-(tributylstannanyl)propan-1-amine

Chemical Property:

Vapor Pressure:1.81E-05mmHg at 25°C
Boiling Point:363.4°Cat760mmHg
Flash Point:173.6°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N,N-dimethyl-3-(tributylstannanyl)propan-1-amine

There total 5 articles about N,N-dimethyl-3-(tributylstannanyl)propan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 40391-95-5
3-(Tributylstannyl)propylamin

: 29346-31-4
tributyl(3-dimethylaminopropyl)tin

Guidance literature:: With HCOOH; CH₂O; In neat (no solvent); Clarke-Eschweiler reductive methylation by addn. of formic acid and formaldehyde (37%) to Sn-compd., mixt. refluxed (80°C, 24 h); cooled to room temp., standard ether-aqueous workup for an amine, elem.anal.;
DOI:10.1016/0022-328X(86)84004-9

Reference yield: 18.1%

: 4226-01-1
tri-n-butyltin lithium

: 109-54-6
3-(Dimethylamino)propyl chloride

: 29346-31-4
tributyl(3-dimethylaminopropyl)tin

Guidance literature:: In tetrahydrofuran; diethyl ether; addn. of tributyltin lithium soln. (prepared in situ from Li and (n-Bu)3SnCl in THF) at -7°C to soln. of the propane in dry ether, mixt.immediately turned white, stirred (2h), refluxed (1h); addn. of water, extd. with CH2Cl2, organic layer dried (MgSO4), evapn. (vac.), bulb to bulb distn. (120°C, 0.1 mmHg) of yellow liq., flash chromy. (Florisil, pentane), addn. of ethylacetate/hexane (2/5);
DOI:10.1016/0022-328X(86)84004-9

Reference yield:

: 5827-70-3
(2-cyanoethyl)tributylstannane

: 29346-31-4
tributyl(3-dimethylaminopropyl)tin

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether

2: HCOOH; CH₂O / neat (no solvent)

With LiAlH₄; HCOOH; CH₂O; In diethyl ether;
DOI:10.1016/0022-328X(86)84004-9