5-Methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole

Base Information

Chemical Name:5-Methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole
CAS No.:89004-17-1
Molecular Formula:C₁₉H₁₈N₂
Molecular Weight:274.365
Hs Code.:
DSSTox Substance ID:DTXSID70520109

Synonyms:89004-17-1;5-Methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole;5h-pyrrolo[1,2-a]imidazole,6,7-dihydro-5-methyl-2,3-diphenyl-;DTXSID70520109

Suppliers and Price of 5-Methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 5-Methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:274.146998583
Heavy Atom Count:21
Complexity:344

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCC2=NC(=C(N12)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 5-Methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole

There total 3 articles about 5-Methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89004-15-9
2-(3-aminobutyl)-4,5-diphenyloxazole

: 89004-17-1
5-methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo<1,2-a>imidazole

Guidance literature:: at 280 ℃; under 5 Torr; Yield given;

Reference yield:

: 89004-09-1
2-(3-oxobutyl)-4,5-diphenyloxazole

: 89004-17-1
5-methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo<1,2-a>imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₃CN, ammonium acetate

2: 280 °C / 5 Torr

With ammonium acetate; sodium cyanoborohydride;

Reference yield:

: 14224-99-8
2-methyl-4,5-diphenyloxazole

: 89004-17-1
5-methyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolo<1,2-a>imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) -78 deg C -> room temperature

2: 49 percent / NaBH₃CN, NH₄OAc / methanol / 4 h / Heating

3: 280 °C / 5 Torr

With n-butyllithium; ammonium acetate; sodium cyanoborohydride; In methanol;