4-Chloro-N-(2-oxopropyl)benzamide

Base Information

Chemical Name:4-Chloro-N-(2-oxopropyl)benzamide
CAS No.:89007-01-2
Molecular Formula:C10H10ClNO2
Molecular Weight:211.648
Hs Code.:
DSSTox Substance ID:DTXSID80604429
Wikidata:Q82502360

Synonyms:89007-01-2;Benzamide, 4-chloro-N-(2-oxopropyl)-;4-Chloro-N-(2-oxopropyl)benzamide;SCHEMBL11004530;DTXSID80604429;AKOS002681477

Suppliers and Price of 4-Chloro-N-(2-oxopropyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-Chloro-N-(2-oxopropyl)benzamide

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:211.0400063
Heavy Atom Count:14
Complexity:222

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)CNC(=O)C1=CC=C(C=C1)Cl

Technology Process of 4-Chloro-N-(2-oxopropyl)benzamide

There total 4 articles about 4-Chloro-N-(2-oxopropyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₂₀H₂₀Cl₂N₂O₂

: 89007-01-2
N-acetonyl-4-chlorobenzamide

Guidance literature:: C₂₀H₂₀Cl₂N₂O₂; With ozone; In methanol; dichloromethane; at -98 ℃; for 0.25h;

With dimethylsulfide; In methanol; dichloromethane; for 1h; Inert atmosphere;
DOI:10.1246/cl.170970

Reference yield: 70.0%

: 947823-35-0
4-chloro-N-(2-hydroxypropyl)benzamide

: 89007-01-2
N-acetonyl-4-chlorobenzamide

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2007.10.007

Reference yield:

: 895-84-1
N,N'-bis(p-chlorobenzoyl)hydrazine

: 89007-01-2
N-acetonyl-4-chlorobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; tert-butylhypochlorite / dichloromethane / 1 h / 0 °C

2.1: silver trifluoromethanesulfonate / dichloromethane / Inert atmosphere

3.1: samarium diiodide / tetrahydrofuran; tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

4.1: ozone / methanol; dichloromethane / 0.25 h / -98 °C

4.2: 1 h / Inert atmosphere

With pyridine; samarium diiodide; tert-butylhypochlorite; silver trifluoromethanesulfonate; ozone; In tetrahydrofuran; methanol; dichloromethane; tert-butyl alcohol; 2.1: |Diels-Alder Cycloaddition;
DOI:10.1246/cl.170970