1-[(Benzenesulfonyl)(methoxy)methyl]cyclohexan-1-ol

Base Information

Chemical Name:1-[(Benzenesulfonyl)(methoxy)methyl]cyclohexan-1-ol
CAS No.:89036-94-2
Molecular Formula:C14H20O4S
Molecular Weight:284.376
Hs Code.:
DSSTox Substance ID:DTXSID00528936

Synonyms:89036-94-2;1-[(Benzenesulfonyl)(methoxy)methyl]cyclohexan-1-ol;DTXSID00528936

Suppliers and Price of 1-[(Benzenesulfonyl)(methoxy)methyl]cyclohexan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-[(Benzenesulfonyl)(methoxy)methyl]cyclohexan-1-ol

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:284.10823029
Heavy Atom Count:19
Complexity:373

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC(C1(CCCCC1)O)S(=O)(=O)C2=CC=CC=C2

Technology Process of 1-[(Benzenesulfonyl)(methoxy)methyl]cyclohexan-1-ol

There total 3 articles about 1-[(Benzenesulfonyl)(methoxy)methyl]cyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 15251-78-2
phenyl methoxymethyl sulfone

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 89036-94-2
1-(Benzenesulfonyl-methoxy-methyl)-cyclohexanol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 15 min, 2.) -78 deg C, 30 min;
DOI:10.1039/a703073h

Reference yield:

: 13865-50-4
methoxymethyl phenyl sulfide

: 89036-94-2
1-(Benzenesulfonyl-methoxy-methyl)-cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / aq. Oxone / methanol / 1.) 5 deg C, 1 h, 2.) r.t., 3 h

2: 83 percent / BuLi / hexane; tetrahydrofuran / 1.) -78 deg C, 15 min, 2.) -78 deg C, 30 min

With Oxone; n-butyllithium; In tetrahydrofuran; methanol; hexane;
DOI:10.1039/a703073h

Reference yield:

: 108-98-5
thiophenol

: 89036-94-2
1-(Benzenesulfonyl-methoxy-methyl)-cyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / t-potassium butoxide / dimethylformamide / 1.) r.t., 1 h, 2.) 3 h

2: 89 percent / aq. Oxone / methanol / 1.) 5 deg C, 1 h, 2.) r.t., 3 h

3: 83 percent / BuLi / hexane; tetrahydrofuran / 1.) -78 deg C, 15 min, 2.) -78 deg C, 30 min

With Oxone; n-butyllithium; potassium tert-butylate; In tetrahydrofuran; methanol; hexane; N,N-dimethyl-formamide;
DOI:10.1039/a703073h