2-Azetidinone, 1-(4-chlorobutyl)-4-phenyl-

Base Information

Chemical Name:2-Azetidinone, 1-(4-chlorobutyl)-4-phenyl-
CAS No.:89044-72-4
Molecular Formula:C13H16ClNO
Molecular Weight:237.729
Hs Code.:
DSSTox Substance ID:DTXSID70473181

Synonyms:2-Azetidinone, 1-(4-chlorobutyl)-4-phenyl-;89044-72-4;DTXSID70473181

Suppliers and Price of 2-Azetidinone, 1-(4-chlorobutyl)-4-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Azetidinone, 1-(4-chlorobutyl)-4-phenyl-

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:237.0920418
Heavy Atom Count:16
Complexity:238

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C(N(C1=O)CCCCCl)C2=CC=CC=C2

Technology Process of 2-Azetidinone, 1-(4-chlorobutyl)-4-phenyl-

There total 3 articles about 2-Azetidinone, 1-(4-chlorobutyl)-4-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6940-78-9
4-chlorobutyl bromide

: 5661-55-2
4-phenylazetidin-2-one

: 89044-72-4
N-(4-chlorobutyl)-4-phenylazetidin-2-one

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1039/c39830000959

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 89044-72-4
N-(4-chlorobutyl)-4-phenylazetidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / diethyl ether / 1 h / Ambient temperature

2: 88 percent / 25percent aq. sodium sulfite, 10percent aq. KOH / diethyl ether; CHCl₃ / 1 h

3: 69 percent / KOH, DMSO / 23 h

With potassium hydroxide; dimethyl sulfoxide; sodium sulfite; In diethyl ether; chloroform;

Reference yield:

: 52341-70-5
N-chlorosulfonyl-4-phenylazetidin-2-one

: 89044-72-4
N-(4-chlorobutyl)-4-phenylazetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / 25percent aq. sodium sulfite, 10percent aq. KOH / diethyl ether; CHCl₃ / 1 h

2: 69 percent / KOH, DMSO / 23 h

With potassium hydroxide; dimethyl sulfoxide; sodium sulfite; In diethyl ether; chloroform;