N-[3-(Benzyloxy)-4-nitrophenyl]acetamide

Base Information

Chemical Name:N-[3-(Benzyloxy)-4-nitrophenyl]acetamide
CAS No.:89102-04-5
Molecular Formula:C15H14N2O4
Molecular Weight:286.287
Hs Code.:
DSSTox Substance ID:DTXSID20556817
Wikidata:Q82438514

Synonyms:89102-04-5;N-[3-(Benzyloxy)-4-nitrophenyl]acetamide;DTXSID20556817

Suppliers and Price of N-[3-(Benzyloxy)-4-nitrophenyl]acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-[3-(Benzyloxy)-4-nitrophenyl]acetamide

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:286.09535693
Heavy Atom Count:21
Complexity:363

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)NC1=CC(=C(C=C1)[N+](=O)[O-])OCC2=CC=CC=C2

Technology Process of N-[3-(Benzyloxy)-4-nitrophenyl]acetamide

There total 4 articles about N-[3-(Benzyloxy)-4-nitrophenyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 712-34-5
3-hydroxy-4-nitroacetanilide

: 100-44-7
benzyl chloride

: 89102-04-5
3-(benzyloxy)-4-nitroacetanilide

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; for 4h; Ambient temperature;
DOI:10.1021/jo00256a036

Reference yield:

: 6317-89-1
3-acetamidophenyl acetate

: 89102-04-5
3-(benzyloxy)-4-nitroacetanilide

Guidance literature:: Multi-step reaction with 3 steps

1: 42 percent / nitric acid / 3 h / -15 - -10 °C

2: 98 percent / K₂CO₃, methanol / 5 h / Ambient temperature

3: 98 percent / K₂CO₃, KI / dimethylformamide / 4 h / Ambient temperature

With methanol; nitric acid; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1021/jo00256a036

Reference yield:

: 89102-03-4
3-acetoxy-4-nitroacetanilide

: 89102-04-5
3-(benzyloxy)-4-nitroacetanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃, methanol / 5 h / Ambient temperature

2: 98 percent / K₂CO₃, KI / dimethylformamide / 4 h / Ambient temperature

With methanol; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1021/jo00256a036