Technology Process of 2H-1,2,3-Triazole-4-carboxylic acid,
5-(2,3-dihydro-1H-benzimidazol-2-yl)-2-(4-methylphenyl)-, hydrazide
There total 6 articles about 2H-1,2,3-Triazole-4-carboxylic acid,
5-(2,3-dihydro-1H-benzimidazol-2-yl)-2-(4-methylphenyl)-, hydrazide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1 h / Heating
2: hydrazine hydrate / methanol / Ambient temperature
3: sodium metaperiodate / H2O / 6 h
4: acetic acid / methanol / 3 h / Heating
With
sodium periodate; hydrazine hydrate; acetic acid;
In
methanol; water;
DOI:10.1016/0008-6215(83)88358-X
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydroxylamine hydrochloride, sodium acetate / ethanol / 3 h / Heating
2: 1 h / Heating
3: hydrazine hydrate / methanol / Ambient temperature
4: sodium metaperiodate / H2O / 6 h
5: acetic acid / methanol / 3 h / Heating
With
sodium periodate; hydroxylamine hydrochloride; sodium acetate; hydrazine hydrate; acetic acid;
In
methanol; ethanol; water;
DOI:10.1016/0008-6215(83)88358-X
- Guidance literature:
-
Multi-step reaction with 6 steps
1: H2O; ethanol / 72 h / Ambient temperature
2: hydroxylamine hydrochloride, sodium acetate / ethanol / 3 h / Heating
3: 1 h / Heating
4: hydrazine hydrate / methanol / Ambient temperature
5: sodium metaperiodate / H2O / 6 h
6: acetic acid / methanol / 3 h / Heating
With
sodium periodate; hydroxylamine hydrochloride; sodium acetate; hydrazine hydrate; acetic acid;
In
methanol; ethanol; water;
DOI:10.1016/0008-6215(83)88358-X
