Bis[2-(4-methylbenzene-1-sulfonyl)cyclohexyl]diselane

Base Information

• Chemical Name: Bis[2-(4-methylbenzene-1-sulfonyl)cyclohexyl]diselane
• CAS No.: 89165-54-8
• Molecular Formula: C₂₆H₃₄O₄S₂Se₂
• Molecular Weight: 632.606
• DSSTox Substance ID: DTXSID20533406
• Mol file: 89165-54-8.mol

Synonyms:89165-54-8;Bis[2-(4-methylbenzene-1-sulfonyl)cyclohexyl]diselane;DTXSID20533406

Chemical Property of Bis[2-(4-methylbenzene-1-sulfonyl)cyclohexyl]diselane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 634.02290
• Heavy Atom Count: 34
• Complexity: 776

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)S(=O)(=O)C2CCCCC2[Se][Se]C3CCCCC3S(=O)(=O)C4=CC=C(C=C4)C

Technology Process of Bis[2-(4-methylbenzene-1-sulfonyl)cyclohexyl]diselane

There total 1 articles about Bis[2-(4-methylbenzene-1-sulfonyl)cyclohexyl]diselane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(p-tolylsulfonyl)selenide (60513-62-4) + cyclohexene (110-83-8) → trans-Se-2-(p-tolylsulfonyl)cyclohexyl p-tolueneselenosulfonate (89165-55-9) + trans-bis(2-(p-tolylsulfonyl)cyclohexyl)diselenide (89165-54-8)

Guidance literature:

In tetrachloromethane; for 1.5h; Irradiation;

DOI:10.1021/jo00183a006

Reference yield:

trans-bis(2-(p-tolylsulfonyl)cyclohexyl)diselenide (89165-54-8) → C13H17BrO2SSe

Guidance literature:

In chloroform;

DOI:10.1021/jo00183a006

Reference yield:

trans-bis(2-(p-tolylsulfonyl)cyclohexyl)diselenide (89165-54-8) → trans-2-(p-tolylsulfonyl)cyclohexyl selenocyanate (89165-56-0)

Guidance literature:

Multi-step reaction with 2 steps

1: CHCl₃

2: CHCl₃; ethanol

In ethanol; chloroform;

DOI:10.1021/jo00183a006

upstream raw materials:

bis(p-tolylsulfonyl)selenide

cyclohexene

Downstream raw materials:

trans-2-(p-tolylsulfonyl)cyclohexyl selenocyanate