(2-benzoyl-4-chloro-6-methyl-phenyl) carbamate

Base Information

• Chemical Name: (2-benzoyl-4-chloro-6-methyl-phenyl) carbamate
• CAS No.: 81393-21-7
• Molecular Formula: C15H12 Cl N O3
• Molecular Weight: 0
• Mol file: 81393-21-7.mol

Synonyms:NSC 359689

Chemical Property of (2-benzoyl-4-chloro-6-methyl-phenyl) carbamate

Chemical Property:

• Vapor Pressure: 1.27E-10mmHg at 25°C
• Boiling Point: 512.6°C at 760 mmHg
• Flash Point: 263.8°C
• PSA: 69.39000
• Density: 1.313g/cm³
• LogP: 4.03720

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-benzoyl-4-chloro-6-methyl-phenyl) carbamate

There total 1 articles about (2-benzoyl-4-chloro-6-methyl-phenyl) carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

isocyanate de chlorosulfonyle (1189-71-5) + (5-Chloro-2-hydroxy-3-methyl-phenyl)-phenyl-methanone → Carbamic acid 2-benzoyl-4-chloro-6-methyl-phenyl ester (81393-21-7)

Guidance literature:

In dichloromethane; for 2h; Ambient temperature;

Reference yield: 66.0%

Carbamic acid 2-benzoyl-4-chloro-6-methyl-phenyl ester (81393-21-7) → 6-Chloro-8-methyl-4-phenyl-benzo[e][1,3]oxazin-2-one (115438-17-0)

Guidance literature:

In ethanol; water; at 20 - 22 ℃; for 12h; rat liver microsomes, pH 7.4;

DOI:10.1021/jo00252a045

upstream raw materials:

isocyanate de chlorosulfonyle

Downstream raw materials:

6-Chloro-8-methyl-4-phenyl-benzo[e][1,3]oxazin-2-one

Refernces