5H-Pyrrolo[3,2-d]pyrimidine-5-carboxylic acid, 4-(ethylthio)-2-phenyl-7-[4-[(phenylmethoxy)methyl]-1,3-dioxolan-2-yl]-, phenylmethyl ester, cis-

Base Information

Chemical Name:5H-Pyrrolo[3,2-d]pyrimidine-5-carboxylic acid, 4-(ethylthio)-2-phenyl-7-[4-[(phenylmethoxy)methyl]-1,3-dioxolan-2-yl]-, phenylmethyl ester, cis-
CAS No.:89193-83-9
Molecular Formula:C₃₃H₃₁N₃O₅S
Molecular Weight:581.692
Hs Code.:

5H-Pyrrolo[3,2-d]pyrimidine-5-carboxylic acid,
4-(ethylthio)-2-phenyl-7-[4-[(phenylmethoxy)methyl]-1,3-dioxolan-2-yl]-,
phenylmethyl ester, cis-

Synonyms:

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Chemical Property of 5H-Pyrrolo[3,2-d]pyrimidine-5-carboxylic acid, 4-(ethylthio)-2-phenyl-7-[4-[(phenylmethoxy)methyl]-1,3-dioxolan-2-yl]-, phenylmethyl ester, cis-

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MSDS Files:: SDS file from LookChem

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Technology Process of 5H-Pyrrolo[3,2-d]pyrimidine-5-carboxylic acid, 4-(ethylthio)-2-phenyl-7-[4-[(phenylmethoxy)methyl]-1,3-dioxolan-2-yl]-, phenylmethyl ester, cis-

There total 6 articles about 5H-Pyrrolo[3,2-d]pyrimidine-5-carboxylic acid, 4-(ethylthio)-2-phenyl-7-[4-[(phenylmethoxy)methyl]-1,3-dioxolan-2-yl]-, phenylmethyl ester, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89177-10-6
3-formyl-5-phenyl-7-ethylthiopyrrolo<3,2-d>pyrimidine

: 89177-15-1,89193-83-9
trans-2-(1-benzyloxycarbonyl-5-phenyl-7-ethylthiopyrrolo<3,2-d>pyrimidin-3-yl)-4-benzyloxymethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / triethylamine / tetrahydrofuran / 1) 3-5 deg C, 0.5 h; 2) room temperature, 2 h

2: p-toluenesulfonic acid / benzene / Heating

With toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; benzene;
DOI:10.1007/BF00515354

Reference yield:

: 89177-10-6
3-formyl-5-phenyl-7-ethylthiopyrrolo<3,2-d>pyrimidine

: 89177-15-1,89193-83-9
cis-2-(1-benzyloxycarbonyl-5-phenyl-7-ethylthiopyrrolo<3,2-d>pyrimidin-3-yl)-4-benzyloxymethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / triethylamine / tetrahydrofuran / 1) 3-5 deg C, 0.5 h; 2) room temperature, 2 h

2: p-toluenesulfonic acid / benzene / Heating

With toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; benzene;
DOI:10.1007/BF00515354

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 89177-15-1,89193-83-9
trans-2-(1-benzyloxycarbonyl-5-phenyl-7-ethylthiopyrrolo<3,2-d>pyrimidin-3-yl)-4-benzyloxymethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / triethylamine / tetrahydrofuran / 1) 3-5 deg C, 0.5 h; 2) room temperature, 2 h

2: p-toluenesulfonic acid / benzene / Heating

With toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; benzene;
DOI:10.1007/BF00515354