2-Butyl-5,6-dihydro[1,1'-biphenyl]-3(4H)-one

Base Information

Chemical Name:2-Butyl-5,6-dihydro[1,1'-biphenyl]-3(4H)-one
CAS No.:89228-96-6
Molecular Formula:C16H20O
Molecular Weight:228.334
Hs Code.:
DSSTox Substance ID:DTXSID90528960
Nikkaji Number:J1.163.007C
Wikidata:Q82398998

Synonyms:89228-96-6;2-Butyl-5,6-dihydro[1,1'-biphenyl]-3(4H)-one;DTXSID90528960

Suppliers and Price of 2-Butyl-5,6-dihydro[1,1'-biphenyl]-3(4H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Butyl-5,6-dihydro[1,1'-biphenyl]-3(4H)-one

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:228.151415257
Heavy Atom Count:17
Complexity:295

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCC1=C(CCCC1=O)C2=CC=CC=C2

Technology Process of 2-Butyl-5,6-dihydro[1,1'-biphenyl]-3(4H)-one

There total 9 articles about 2-Butyl-5,6-dihydro[1,1'-biphenyl]-3(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: ((2′-butyl-3′-phenyl-[1,1′-bi(cyclopropan)]-2′-en-1-yl)oxy)triisopropylsilane

: 89228-96-6
2-butyl-3-phenyl-2-cyclohexenone

Guidance literature:: ((2′-butyl-3′-phenyl-[1,1′-bi(cyclopropan)]-2′-en-1-yl)oxy)triisopropylsilane; With zinc(II) iodide; In 1,2-dichloro-ethane; at 70 ℃; for 12h; Schlenk technique; Inert atmosphere;

With water; In cis-1,2-Dichloroethylene; at 70 - 110 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo5010923

Reference yield: 74.0%

: 73172-56-2
ethyl 4-benzoylbutanoate

: 204571-41-5
ethyl α,α-dibromocaproate

: 89228-96-6
2-butyl-3-phenyl-2-cyclohexenone

: ethyl 5-phenyl-5-decenoate

Guidance literature:: ethyl α,α-dibromocaproate; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 - 0 ℃; for 3.5h;

ethyl 4-benzoylbutanoate; In tetrahydrofuran; pentane; at -78 ℃; for 5h;

With silica gel; In benzene; for 10h; Further stages.; Heating;
DOI:10.1021/jo015929w

Reference yield:

: 73172-56-2
ethyl 4-benzoylbutanoate

: 89228-96-6
2-butyl-3-phenyl-2-cyclohexenone

Guidance literature:: Multi-step reaction with 2 steps

1: pentane; tetrahydrofuran / -78 °C

2: SiO₂ / benzene / Heating

With silica gel; In tetrahydrofuran; pentane; benzene;
DOI:10.1021/ja990656w