3-Bromo-2-cyanopyridine

Base Information

Chemical Name:3-Bromo-2-cyanopyridine
CAS No.:55758-02-6
Molecular Formula:C6H3BrN2
Molecular Weight:183.007
Hs Code.:29333990
European Community (EC) Number:624-977-3
DSSTox Substance ID:DTXSID70355837
Nikkaji Number:J734.422H
Wikidata:Q72453864
Mol file:55758-02-6.mol

Synonyms:3-Bromo-2-cyanopyridine;55758-02-6;3-bromopyridine-2-carbonitrile;3-bromopicolinonitrile;2-cyano-3-bromopyridine;3-bromo-2-pyridinecarbonitrile;2-Pyridinecarbonitrile, 3-bromo-;MFCD02683288;3-Bromo-pyridine-2-carbonitrile;3-bromopicolino-nitrile;Bromo-2-cyano-pyridine;3-bromo-2-cyano-pyridine;3-Bromo-pyridin-2-nitrile;SCHEMBL391339;HCOPIUVJCIZALB-UHFFFAOYSA-;DTXSID70355837;HCOPIUVJCIZALB-UHFFFAOYSA-N;BBL100455;CL0159;STL554249;3-Bromopyridine-2-carbonitrile, 97%;AKOS005145804;AC-1874;CS-W002967;FS-2428;HY-W002967;PB24769;BP-10221;SY003790;A8051;AM20070188;B4382;FT-0650468;EN300-102904;AC-907/34104040;W-203110;InChI=1/C6H3BrN2/c7-5-2-1-3-9-6(5)4-8/h1-3H

Suppliers and Price of 3-Bromo-2-cyanopyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
3-Bromo-2-cyanopyridine
1g
$ 382.00

TRC
3-Bromo-2-cyanopyridine
25g
$ 100.00

TRC
3-Bromo-2-cyanopyridine
5g
$ 50.00

TCI Chemical
3-Bromo-2-cyanopyridine >98.0%(GC)
1g
$ 40.00

TCI Chemical
3-Bromo-2-cyanopyridine >98.0%(GC)
5g
$ 116.00

SynQuest Laboratories
3-Bromopyridine-2-carbonitrile 97.0%
25 g
$ 162.00

SynQuest Laboratories
3-Bromopyridine-2-carbonitrile 97.0%
1 g
$ 21.00

SynQuest Laboratories
3-Bromopyridine-2-carbonitrile 97.0%
5 g
$ 71.00

SynChem
3-Bromo-pyridine-2-carbonitrile 95+%
1 g
$ 30.00

SynChem
3-Bromo-pyridine-2-carbonitrile 95+%
5 g
$ 85.00

Total 119 raw suppliers

Chemical Property of 3-Bromo-2-cyanopyridine

Chemical Property:

Appearance/Colour:slight yellow powder
Vapor Pressure:0.00153mmHg at 25°C
Melting Point:98.2-99.0 °C
Refractive Index:1.611
Boiling Point:295.4 °C at 760 mmHg
PKA:-2.68±0.10(Predicted)
Flash Point:132.4 °C
PSA：36.68000
Density:1.72 g/cm³
LogP:1.71578
Storage Temp.:-20?C Freezer, Under Inert Atmosphere
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:181.94796
Heavy Atom Count:9
Complexity:137

Purity/Quality:

98% ^*data from raw suppliers

3-Bromo-2-cyanopyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi,Xn
Hazard Codes:Xi,Xn
Statements: 22-37/38-41
Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:C1=CC(=C(N=C1)C#N)Br

Technology Process of 3-Bromo-2-cyanopyridine

There total 3 articles about 3-Bromo-2-cyanopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 626-55-1,163928-56-1
3-Bromopyridine

: 7677-24-9
trimethylsilyl cyanide

: 55758-02-6
3-bromopyridine-2-carbonitrile

: 13958-98-0
3-bromo-4-cyanopyridine

: 97483-77-7
2-Cyano-5-bromopyridine

Guidance literature:: 3-Bromopyridine; With trifluoromethylsulfonic anhydride; In chloroform; at 20 ℃; for 1h; Inert atmosphere; Sealed tube;

trimethylsilyl cyanide; In chloroform; at 60 ℃; for 3h; Inert atmosphere; Sealed tube;

With 4-methyl-morpholine; In chloroform; at 60 ℃; for 17h; Overall yield = 79 %; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201703931