Ethyl 4-(2-oxocyclohexyl)pyridine-1(4H)-carboxylate

Base Information

Chemical Name:Ethyl 4-(2-oxocyclohexyl)pyridine-1(4H)-carboxylate
CAS No.:89318-16-1
Molecular Formula:C₁₄H₁₉NO₃
Molecular Weight:249.31
Hs Code.:
DSSTox Substance ID:DTXSID10519618

Synonyms:89318-16-1;Ethyl 4-(2-oxocyclohexyl)pyridine-1(4H)-carboxylate;DTXSID10519618

Suppliers and Price of Ethyl 4-(2-oxocyclohexyl)pyridine-1(4H)-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 4-(2-oxocyclohexyl)pyridine-1(4H)-carboxylate

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:249.13649347
Heavy Atom Count:18
Complexity:373

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)N1C=CC(C=C1)C2CCCCC2=O

Technology Process of Ethyl 4-(2-oxocyclohexyl)pyridine-1(4H)-carboxylate

There total 4 articles about Ethyl 4-(2-oxocyclohexyl)pyridine-1(4H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 6651-36-1
1-(Trimethylsilyloxy)cyclohexene

: 63755-30-6
N-ethoxycarbonylpyridinium chloride

: 2-(2-Oxo-cyclohexyl)-2H-pyridine-1-carboxylic acid ethyl ester

: 89318-16-1
4-(2-Oxo-cyclohexyl)-4H-pyridine-1-carboxylic acid ethyl ester

: 89318-21-8
4-(2-Trimethylsilanyloxy-cyclohex-1-enyl)-4H-pyridine-1-carboxylic acid ethyl ester

Guidance literature:: In dichloromethane; at 0 ℃; for 9h;
DOI:10.1016/S0040-4039(00)88414-2

Reference yield:

: 110-86-1
pyridine

: 89318-16-1
4-(2-Oxo-cyclohexyl)-4H-pyridine-1-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 42 percent / CH₂Cl₂ / 9 h / 0 °C

In dichloromethane;
DOI:10.1016/S0040-4039(00)88414-2