Silane, trimethyl[1-phenyl-2-(phenylsulfonyl)ethyl]-

Base Information

Chemical Name:Silane, trimethyl[1-phenyl-2-(phenylsulfonyl)ethyl]-
CAS No.:89333-88-0
Molecular Formula:C17H22O2SSi
Molecular Weight:318.512
Hs Code.:
DSSTox Substance ID:DTXSID20443556
Nikkaji Number:J745.803G

Synonyms:Silane, trimethyl[1-phenyl-2-(phenylsulfonyl)ethyl]-;89333-88-0;DTXSID20443556;Phenyl[beta-(trimethylsilyl)phenethyl] sulfone

Suppliers and Price of Silane, trimethyl[1-phenyl-2-(phenylsulfonyl)ethyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, trimethyl[1-phenyl-2-(phenylsulfonyl)ethyl]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:318.11097765
Heavy Atom Count:21
Complexity:407

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C(CS(=O)(=O)C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of Silane, trimethyl[1-phenyl-2-(phenylsulfonyl)ethyl]-

There total 5 articles about Silane, trimethyl[1-phenyl-2-(phenylsulfonyl)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 122760-30-9
1-phenylthio-2-phenyl-2-trimethylsilylethane

: 89333-88-0
1-phenylsulfonyl-2-phenyl-2-trimethylsilylethane

Guidance literature:: With ammonium heptamolybdate; dihydrogen peroxide; In methanol; at 20 ℃; for 16h;
DOI:10.1039/P19960001511

Reference yield:

: 98-81-7
1-bromovinylbenzene

: 89333-88-0
1-phenylsulfonyl-2-phenyl-2-trimethylsilylethane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg / 1.) THF, 1 h, 2.) reflux, 5 h

2: 86 percent / AIBN / 1 h / 90 °C

3: 65 percent / (NH₄)6Mo₇O₂₄*7H₂O, 30percent H₂O₂ / methanol / 16 h / 20 °C

With ammonium heptamolybdate; 2,2'-azobis(isobutyronitrile); dihydrogen peroxide; magnesium; In methanol;
DOI:10.1039/P19960001511

Reference yield:

: 1923-01-9
trimethyl(1-phenylvinyl)silane

: 89333-88-0
1-phenylsulfonyl-2-phenyl-2-trimethylsilylethane

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / AIBN / 1 h / 90 °C

2: 65 percent / (NH₄)6Mo₇O₂₄*7H₂O, 30percent H₂O₂ / methanol / 16 h / 20 °C

With ammonium heptamolybdate; 2,2'-azobis(isobutyronitrile); dihydrogen peroxide; In methanol;
DOI:10.1039/P19960001511