3-Bromo-4-(diphenylphosphoryl)-3-methylbutan-2-ol

Base Information

Chemical Name:3-Bromo-4-(diphenylphosphoryl)-3-methylbutan-2-ol
CAS No.:89358-76-9
Molecular Formula:C₁₇H₂₀BrO₂P
Molecular Weight:367.222
Hs Code.:
DSSTox Substance ID:DTXSID20527204

Synonyms:89358-76-9;3-Bromo-4-(diphenylphosphoryl)-3-methylbutan-2-ol;DTXSID20527204

Suppliers and Price of 3-Bromo-4-(diphenylphosphoryl)-3-methylbutan-2-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-Bromo-4-(diphenylphosphoryl)-3-methylbutan-2-ol

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:366.03843
Heavy Atom Count:21
Complexity:353

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C(C)(CP(=O)(C1=CC=CC=C1)C2=CC=CC=C2)Br)O

Technology Process of 3-Bromo-4-(diphenylphosphoryl)-3-methylbutan-2-ol

There total 4 articles about 3-Bromo-4-(diphenylphosphoryl)-3-methylbutan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 69803-63-0
1-diphenylphosphinoyl-2-methyl-2,3-epoxybutane

: 89358-76-9
2-bromo-1-diphenylphosphinoyl-2-methylbutan-3-ol

Guidance literature:: With magnesium bromide; In benzene; for 20h; Heating;

Reference yield:

: 57984-58-4
(E)-(2-methylbut-2-enyl)diphenylphosphine oxide

: 89358-76-9
2-bromo-1-diphenylphosphinoyl-2-methylbutan-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂CO₃, MCPBA / CH₂Cl₂ / 96 h / Ambient temperature

2: 12 percent / MgBr₂ / benzene / 20 h / Heating

With sodium carbonate; 3-chloro-benzenecarboperoxoic acid; magnesium bromide; In dichloromethane; benzene;

Reference yield:

: 160882-66-6
1-(Diphenyl-phosphinoyl)-2-methyl-butan-2-ol

: 89358-76-9
2-bromo-1-diphenylphosphinoyl-2-methylbutan-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: TFA / 1 h / Heating

2: Na₂CO₃, MCPBA / CH₂Cl₂ / 96 h / Ambient temperature

3: 12 percent / MgBr₂ / benzene / 20 h / Heating

With sodium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; magnesium bromide; In dichloromethane; benzene;