(2-Benzylphenyl)(naphthalen-2-yl)methanone

Base Information

• Chemical Name: (2-Benzylphenyl)(naphthalen-2-yl)methanone
• CAS No.: 7424-65-9
• Molecular Formula: C24H18O
• Molecular Weight: 322.3991
• NSC Number: 99513
• DSSTox Substance ID: DTXSID40295074
• Wikidata: Q82034762

Synonyms:(2-benzylphenyl)(naphthalen-2-yl)methanone;7424-65-9;NSC99513;DTXSID40295074;NSC-99513

Chemical Property of (2-Benzylphenyl)(naphthalen-2-yl)methanone

Chemical Property:

• Vapor Pressure: 3.32E-11mmHg at 25°C
• Boiling Point: 527.2°Cat760mmHg
• Flash Point: 232.2°C
• Density: 1.147g/cm³
• XLogP3: 6.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 322.135765193
• Heavy Atom Count: 25
• Complexity: 435

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CC2=CC=CC=C2C(=O)C3=CC4=CC=CC=C4C=C3

Technology Process of (2-Benzylphenyl)(naphthalen-2-yl)methanone

There total 1 articles about (2-Benzylphenyl)(naphthalen-2-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1-(naphthalen-2-yl)-2-phenylethanone (1762-15-8) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → (2-benzyl-phenyl)-[2]naphthyl ketone (7424-65-9)

Guidance literature:

With cesium fluoride; In 1,2-dimethoxyethane; at 20 ℃; for 14h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.orglett.6b00578

Reference yield:

(2-benzyl-phenyl)-[2]naphthyl ketone (7424-65-9) → 12-phenyl-benz[a]anthracene (7424-73-9)

Guidance literature:

With zinc; at 430 ℃;

DOI:10.1021/jo01341a004

Reference yield:

(2-benzyl-phenyl)-[2]naphthyl ketone (7424-65-9) → 9-(naphthyl-2-yl)anthracene (7424-72-8)

Guidance literature:

With hydrogen bromide; acetic acid; at 180 ℃;

DOI:10.1021/ja01540a051

upstream raw materials:

1-(naphthalen-2-yl)-2-phenylethanone

2-(trimethylsilyl)phenyl trifluoromethanesulfonate

Downstream raw materials:

9-(naphthyl-2-yl)anthracene

12-phenyl-benz[a]anthracene

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