4-AMINO-N-ETHYLBENZAMIDE

Base Information

• Chemical Name: 4-AMINO-N-ETHYLBENZAMIDE
• CAS No.: 89399-17-7
• Molecular Formula: C9H12N2O
• Molecular Weight: 164.207
• Hs Code.: 2924299090
• Mol file: 89399-17-7.mol

Synonyms:Benzamide,4-amino-N-ethyl;4-amino-ethyl-benzamide;4-Amino-N-aethyl-benzamid;4-amino-benzoic acid ethylamide;4-Amino-benzoesaeure-aethylamid;

Chemical Property of 4-AMINO-N-ETHYLBENZAMIDE

Chemical Property:

• Vapor Pressure: 1.15E-05mmHg at 25°C
• Boiling Point: 369.9oC at 760 mmHg
• Flash Point: 177.5oC
• PSA: 55.12000
• Density: 1.105g/cm3
• LogP: 1.99060

Purity/Quality:

97% ^*data from raw suppliers

4-Amino-N-ethylbenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-AMINO-N-ETHYLBENZAMIDE

There total 6 articles about 4-AMINO-N-ETHYLBENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N-ethyl-4-nitrobenzamide (50445-50-6) → 4-amino-N-ethylbenzamide (89399-17-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 3h; under 2327.2 Torr;

DOI:10.1021/jm00372a013

Reference yield:

4-nitro-benzoyl chloride (122-04-3) → 4-amino-N-ethylbenzamide (89399-17-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / 20percent (w/v) K₂CO₃ / tetrahydrofuran / 12 h / Heating

2: 80 percent / H₂ / 5percent Pd/C / ethanol / 3 h / 2327.2 Torr

With hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol;

DOI:10.1021/jm00372a013

Reference yield:

4-Boc-amino-N-ethylbenzamide → 4-amino-N-ethylbenzamide (89399-17-7)

Guidance literature:

With chlorotriisopropylsilane; trifluoroacetic acid; at 20 ℃; for 3h;

DOI:10.1021/jm049637+

upstream raw materials:

N-ethyl-4-nitrobenzamide

4-(N-tert-butoxycarbonyl)aminobenzoic acid

4-nitro-benzoyl chloride

4-nitro-benzoic acid