2,3-Dimethoxy-5-methylbenzaldehyde

Base Information

Chemical Name:2,3-Dimethoxy-5-methylbenzaldehyde
CAS No.:5701-86-0
Molecular Formula:C10H12O3
Molecular Weight:180.20
Hs Code.:2912499000
DSSTox Substance ID:DTXSID80470242
Nikkaji Number:J2.287.117J
Wikidata:Q72468016
Mol file:5701-86-0.mol

Synonyms:2,3-Dimethoxy-5-methylbenzaldehyde;5701-86-0;2,3-dimethoxy-5-methyl-benzaldehyde;SCHEMBL13452129;DTXSID80470242;2,3-Dimethoxy-5-methylbenzaldehyd;AKOS006229943;AB39380;Benzaldehyde, 2,3-dimethoxy-5-methyl-;AC-23857;AM20080610;CS-0247912;FT-0762126;EN300-378437;A831283

Suppliers and Price of 2,3-Dimethoxy-5-methylbenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,3-DIMETHOXY-5-METHYLBENZALDEHYDE 95.00%
5MG
$ 495.03

AK Scientific
2,3-Dimethoxy-5-methylbenzaldehyde
2.5g
$ 1404.00

AK Scientific
2,3-Dimethoxy-5-methylbenzaldehyde
1g
$ 764.00

AK Scientific
2,3-Dimethoxy-5-methylbenzaldehyde
500mg
$ 618.00

AK Scientific
2,3-Dimethoxy-5-methylbenzaldehyde
250mg
$ 372.00

Total 15 raw suppliers

Chemical Property of 2,3-Dimethoxy-5-methylbenzaldehyde

Chemical Property:

Vapor Pressure:1.41E-11mmHg at 25°C
Melting Point:40 °C
Refractive Index:1.655
Boiling Point:290.328 °C at 760 mmHg
Flash Point:120.192 °C
PSA：35.53000
Density:1.09 g/cm³
LogP:1.82470
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:180.078644241
Heavy Atom Count:13
Complexity:170

Purity/Quality:

98%Min ^*data from raw suppliers

2,3-DIMETHOXY-5-METHYLBENZALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)OC)OC)C=O

Technology Process of 2,3-Dimethoxy-5-methylbenzaldehyde

There total 9 articles about 2,3-Dimethoxy-5-methylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93-51-6
2-Methoxy-4-methylphenol

: 5701-86-0
2,3-dimethoxy-5-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1.1: 95 percent / K₂CO₃ / acetone / 6 h / Heating

2.1: 90 percent / 24 h / 180 °C

3.1: 95 percent / KOH / methanol / 10 h / Heating

4.1: 96 percent / sodium hydroxyde / H₂O / 1 h / Heating

5.1: NaHCO₃; ozone / methanol; CH₂Cl₂ / 0.22 h / -70 °C

5.2: 80 percent / dimethyl sulfide / methanol; CH₂Cl₂ / 8 h / 20 °C

With potassium hydroxide; sodium hydroxide; sodium hydrogencarbonate; potassium carbonate; ozone; In methanol; dichloromethane; water; acetone; 2.1: Claisen rearrangement;
DOI:10.1016/j.tet.2006.01.021

Reference yield:

: 77879-82-4
2-allyl-4-methyl-6-methoxyphenol

: 5701-86-0
2,3-dimethoxy-5-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: 95 percent / KOH / methanol / 10 h / Heating

2.1: 96 percent / sodium hydroxyde / H₂O / 1 h / Heating

3.1: NaHCO₃; ozone / methanol; CH₂Cl₂ / 0.22 h / -70 °C

3.2: 80 percent / dimethyl sulfide / methanol; CH₂Cl₂ / 8 h / 20 °C

With potassium hydroxide; sodium hydroxide; sodium hydrogencarbonate; ozone; In methanol; dichloromethane; water;
DOI:10.1016/j.tet.2006.01.021

Reference yield:

: Methyl-(6-hydroxy-3-methyl-5-propenyl-phenyl)-aether

: 5701-86-0
2,3-dimethoxy-5-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / sodium hydroxyde / H₂O / 1 h / Heating

2.1: NaHCO₃; ozone / methanol; CH₂Cl₂ / 0.22 h / -70 °C

2.2: 80 percent / dimethyl sulfide / methanol; CH₂Cl₂ / 8 h / 20 °C

With sodium hydroxide; sodium hydrogencarbonate; ozone; In methanol; dichloromethane; water;
DOI:10.1016/j.tet.2006.01.021