2-(2-Oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one

Base Information

Chemical Name:2-(2-Oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one
CAS No.:89506-40-1
Molecular Formula:C17H14O2
Molecular Weight:250.297
Hs Code.:
DSSTox Substance ID:DTXSID00520399

Synonyms:89506-40-1;2-(2-Oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one;DTXSID00520399

Suppliers and Price of 2-(2-Oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 2-(2-Oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:250.099379685
Heavy Atom Count:19
Complexity:354

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(C(=O)C2=CC=CC=C21)CC(=O)C3=CC=CC=C3

Technology Process of 2-(2-Oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one

There total 8 articles about 2-(2-Oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: methyl 2-(2-oxo-2-phenylethyl)-1-oxoindane-2-carboxylate

: 89506-40-1
2-(2-oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one

Guidance literature:: With lithium iodide monohydrate; In N,N-dimethyl-formamide; at 150 ℃; for 2h;
DOI:10.1002/ejoc.201100289

Reference yield: 51.0%

: 13261-70-6
2-methylidene-2,3-dihydro-1H-inden-1-one

: 100-52-7
benzaldehyde

: 89506-40-1
2-(2-oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one

Guidance literature:: With triethylamine; 3,4-dimethyl-5-(2-hydroxyethyl)thiazolium iodide; In ethanol; at 60 - 90 ℃; for 15h;

Reference yield:

: 67153-85-9
2-dimethylaminomethyl-indan-1-one

: 89506-40-1
2-(2-oxo-2-phenylethyl)-2,3-dihydro-1H-inden-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 41 percent / 48 h / 140 °C

2: 95 percent / 550 °C / 10 Torr

3: 51 percent / NEt₃ / 5-(2-hydroxyethyl)-3,4-dimethyl-1,3-thiazolium iodide / ethanol / 15 h / 60 - 90 °C

With triethylamine; 3,4-dimethyl-5-(2-hydroxyethyl)thiazolium iodide; In ethanol;