1-(3,4-Dichlorophenyl)hydrazine-1-carbonitrile

Base Information

Chemical Name:1-(3,4-Dichlorophenyl)hydrazine-1-carbonitrile
CAS No.:89521-91-5
Molecular Formula:C7H5Cl2N3
Molecular Weight:202.043
Hs Code.:
DSSTox Substance ID:DTXSID40523607
Wikidata:Q82389810

Synonyms:89521-91-5;1-(3,4-Dichlorophenyl)hydrazine-1-carbonitrile;DTXSID40523607

Suppliers and Price of 1-(3,4-Dichlorophenyl)hydrazine-1-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,4-Dichlorophenyl)hydrazine-1-carbonitrile

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:200.9860526
Heavy Atom Count:12
Complexity:200

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1N(C#N)N)Cl)Cl

Technology Process of 1-(3,4-Dichlorophenyl)hydrazine-1-carbonitrile

There total 1 articles about 1-(3,4-Dichlorophenyl)hydrazine-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.5%

: 506-68-3
bromocyane

: 13124-18-0
3,4-dichlorophenylhydrazine

: 89521-91-5
1-(3,4-dichorophenyl)hydrazine-1-carbonitrile

Guidance literature:: With sodium hydroxide; In ethanol; for 20h; Ambient temperature;

Reference yield: 90.0%

: 89521-91-5
1-(3,4-dichorophenyl)hydrazine-1-carbonitrile

: 89521-97-1
2-(3,4-dichlorophenyl)thiosemicarbazide

Guidance literature:: With hydrogen sulfide; triethylamine; In ethanol; at 5 ℃; ice bath, overnight;

Reference yield:

: 89521-91-5
1-(3,4-dichorophenyl)hydrazine-1-carbonitrile

: 89522-07-6
1-(3,4-dichlorophenyl)-3-trifluoromethyl-5-methylthio-1,2,4-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / hydrogen sulfide, triethylamine / ethanol / 5 °C / ice bath, overnight

2: 93 percent / methanol / 2 h / 66 °C / pH=9

3: 85 percent / tetrahydrofuran / 3 h / Heating

With hydrogen sulfide; triethylamine; In tetrahydrofuran; methanol; ethanol;