Methyl 1-(4-chlorophenyl)hydrazine-1-carboximidothioate

Base Information

Chemical Name:Methyl 1-(4-chlorophenyl)hydrazine-1-carboximidothioate
CAS No.:89522-00-9
Molecular Formula:C8H10ClN3S
Molecular Weight:215.706
Hs Code.:
DSSTox Substance ID:DTXSID50523618
Wikidata:Q82389831

Synonyms:89522-00-9;Methyl 1-(4-chlorophenyl)hydrazine-1-carboximidothioate;DTXSID50523618

Suppliers and Price of Methyl 1-(4-chlorophenyl)hydrazine-1-carboximidothioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 1-(4-chlorophenyl)hydrazine-1-carboximidothioate

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:215.0283962
Heavy Atom Count:13
Complexity:180

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CSC(=N)N(C1=CC=C(C=C1)Cl)N

Technology Process of Methyl 1-(4-chlorophenyl)hydrazine-1-carboximidothioate

There total 3 articles about Methyl 1-(4-chlorophenyl)hydrazine-1-carboximidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 89521-94-8
2-(4-chlorophenyl)thiosemicarbazide

: 74-88-4
methyl iodide

: 89522-00-9
2-(4-chlorophenyl)-3-methylisothiosemicarbazide

Guidance literature:: In methanol; at 66 ℃; for 2h; pH=9;

Reference yield:

: 89521-88-0
1-(4-chlorophenyl)hydrazine-1-carbonitrile

: 89522-00-9
2-(4-chlorophenyl)-3-methylisothiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / hydrogen sulfide, triethylamine / ethanol / 5 °C / ice bath, overnight

2: 89 percent / methanol / 2 h / 66 °C / pH=9

With hydrogen sulfide; triethylamine; In methanol; ethanol;

Reference yield:

: 1073-69-4
N-4-chlorophenylhydrazine

: 89522-00-9
2-(4-chlorophenyl)-3-methylisothiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: 26 percent / NaOH / aq. ethanol / 20 h / Ambient temperature

2: 70 percent / hydrogen sulfide, triethylamine / ethanol / 5 °C / ice bath, overnight

3: 89 percent / methanol / 2 h / 66 °C / pH=9

With sodium hydroxide; hydrogen sulfide; triethylamine; In methanol; ethanol;