1,3-Adamantanediol monoacrylate

Base Information

• Chemical Name: 1,3-Adamantanediol monoacrylate
• CAS No.: 115372-36-6
• Molecular Formula: C14H20 O3
• Molecular Weight: 236.31
• Hs Code.: 2916140000
• Mol file: 115372-36-6.mol

Synonyms:1,3-Adamantanediolmonomethacrylate; 1-Methacryloyloxy-3-adamantanol; 3-Hydroxy-1-adamantylmethacrylate; Adamantate HM

Chemical Property of 1,3-Adamantanediol monoacrylate

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 89.0 to 93.0 °C
• Boiling Point: 329 ºC
• PKA: 14.46±0.40(Predicted)
• Flash Point: 133 ºC
• PSA: 46.53000
• Density: 1.17
• LogP: 2.18940
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: soluble in Methanol

Purity/Quality:

99% ^*data from raw suppliers

3-Hydroxy-1-adamantylMethacrylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Adamantanediol monoacrylate

There total 3 articles about 1,3-Adamantanediol monoacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ethylene-methyl methacrylate (93942-70-2) → 3-hydroxy-1-adamantyl methacrylate (115372-36-6)

Guidance literature:

Reference yield:

poly(methacrylic acid) (79-41-4,25087-26-7,50867-57-7) + 1,3-adamantandiol (5001-18-3) → 3-hydroxy-1-adamantyl methacrylate (115372-36-6)

Guidance literature:

With toluene-4-sulfonic acid; In toluene;

Reference yield:

→ 3-hydroxy-1-adamantyl methacrylate (115372-36-6)

Guidance literature:

upstream raw materials:

poly(methacrylic acid)

1,3-adamantandiol

ethylene-methyl methacrylate

Refernces

• 1、 -. "Adamantane derivatives and processes for the preparation thereof". Page column 24-25. . Retrieved 2008/06/13.
• 2、 -. "POLYMERIZABLE ADAMANTANE DERIVATIVES AND PROCESS FOR PRODUCING THE SAME". . . Retrieved 2008/06/13.